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2.0995e-05 9.3311e-06 0 0 0.0072924 2.529e-05 0 2.529e-07 0 0.0072924 +0.0072924 0 0 0 0 0 0 0 1.489473e-05 2.315337e-05 1.081098e-05 5.830274e-05 +0 0 0 0 0 0 0.096602 5.5353 0 0 0 0.00010201 9.3311e-06 0.00059719 0 0 +0 0 2.529e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1995 +##$TE1= 300.1995 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 23696363 +##$YMIN_a= -12622196 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage1/111/fid b/Extracellular/DD/DD_Stage1/111/fid new file mode 100644 index 0000000000000000000000000000000000000000..68558b5eecc100634593fb302c0287f9857e7a2b Binary files /dev/null and b/Extracellular/DD/DD_Stage1/111/fid differ diff --git a/Extracellular/DD/DD_Stage1/111/pdata/.DS_Store b/Extracellular/DD/DD_Stage1/111/pdata/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..99d2a29acf186ca231395c614c259ae9e97452e2 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/111/pdata/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage1/111/pdata/1/1r b/Extracellular/DD/DD_Stage1/111/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..729844b842167dd7730085af4312f1adab6df139 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/111/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage1/111/pdata/1/proc b/Extracellular/DD/DD_Stage1/111/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/111/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1/111/pdata/1/procs b/Extracellular/DD/DD_Stage1/111/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..76a6909489b5e4eca1cce0ab655495f101279e7f --- /dev/null +++ b/Extracellular/DD/DD_Stage1/111/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83982 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909158546 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 281892851 +##$YMIN_p= -70187 +##END= diff --git a/Extracellular/DD/DD_Stage1/111/pdata/1/title b/Extracellular/DD/DD_Stage1/111/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..fe75f2d6fdca3819d88b6894c0a0096b2ec525cc --- /dev/null +++ b/Extracellular/DD/DD_Stage1/111/pdata/1/title @@ -0,0 +1 @@ +111, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1/111/pulseprogram b/Extracellular/DD/DD_Stage1/111/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/111/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1/112/.DS_Store b/Extracellular/DD/DD_Stage1/112/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..8aca75a32ae599da59f47fbf45fafe551b115189 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/112/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage1/112/acqu b/Extracellular/DD/DD_Stage1/112/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage1/112/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) 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300.2017 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 21589330 +##$YMIN_a= -11566992 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage1/112/fid b/Extracellular/DD/DD_Stage1/112/fid new file mode 100644 index 0000000000000000000000000000000000000000..1e9548d73e0e308c4afa40ee3e4f993fafe15760 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/112/fid differ diff --git a/Extracellular/DD/DD_Stage1/112/pdata/.DS_Store b/Extracellular/DD/DD_Stage1/112/pdata/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..011ed9e2e391a2cdda8430c4b8156dc751bc03d5 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/112/pdata/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage1/112/pdata/1/1r b/Extracellular/DD/DD_Stage1/112/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..e167a064f4b2d725e594967fc133254066cdca73 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/112/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage1/112/pdata/1/proc b/Extracellular/DD/DD_Stage1/112/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/112/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1/112/pdata/1/procs b/Extracellular/DD/DD_Stage1/112/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..22c0dae8a84943788b04615af9aa7ecac4f6c9db --- /dev/null +++ b/Extracellular/DD/DD_Stage1/112/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83977 +##$PC= 1 +##$PHC0= -25.34546 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990919355 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 275792005 +##$YMIN_p= -66786 +##END= diff --git a/Extracellular/DD/DD_Stage1/112/pdata/1/title b/Extracellular/DD/DD_Stage1/112/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..860a5676a63df2115ce98aee9ddd2ca50c2c0885 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/112/pdata/1/title @@ -0,0 +1 @@ +112, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1/112/pulseprogram b/Extracellular/DD/DD_Stage1/112/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/112/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1/113/acqu b/Extracellular/DD/DD_Stage1/113/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage1/113/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 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+##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage1/113/fid b/Extracellular/DD/DD_Stage1/113/fid new file mode 100644 index 0000000000000000000000000000000000000000..e1f8d2b2caba93aad182a123f00bbc6ae8d9bf2f Binary files /dev/null and b/Extracellular/DD/DD_Stage1/113/fid differ diff --git a/Extracellular/DD/DD_Stage1/113/pdata/1/1r b/Extracellular/DD/DD_Stage1/113/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..d43fa39eb0483786357741bfcdb875472043ff16 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/113/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage1/113/pdata/1/proc b/Extracellular/DD/DD_Stage1/113/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/113/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1/113/pdata/1/procs b/Extracellular/DD/DD_Stage1/113/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..20932627abc7db287c4c505f1bbf187aefcf2c5b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/113/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8396 +##$PC= 1 +##$PHC0= -25.75745 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990931398 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 323053322 +##$YMIN_p= -76587 +##END= diff --git a/Extracellular/DD/DD_Stage1/113/pdata/1/title b/Extracellular/DD/DD_Stage1/113/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..3e9b72a293cadcbd8fc7d3fb16ba6128dfc98b1c --- /dev/null +++ b/Extracellular/DD/DD_Stage1/113/pdata/1/title @@ -0,0 +1 @@ +113, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1/113/pulseprogram b/Extracellular/DD/DD_Stage1/113/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/113/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1/114/acqu b/Extracellular/DD/DD_Stage1/114/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage1/114/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 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+##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage1/114/fid b/Extracellular/DD/DD_Stage1/114/fid new file mode 100644 index 0000000000000000000000000000000000000000..644739891ad94da4607d3cb596bf6aa0d4c3a5be Binary files /dev/null and b/Extracellular/DD/DD_Stage1/114/fid differ diff --git a/Extracellular/DD/DD_Stage1/114/pdata/1/1r b/Extracellular/DD/DD_Stage1/114/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..c07f94d69d1d13f7764aafb54f49b23fb8ed3454 Binary files /dev/null and b/Extracellular/DD/DD_Stage1/114/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage1/114/pdata/1/proc b/Extracellular/DD/DD_Stage1/114/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/114/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1/114/pdata/1/procs b/Extracellular/DD/DD_Stage1/114/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..0115da01d4eb70d12a8325e0ae4c9fddfc4b0c33 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/114/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83963 +##$PC= 1 +##$PHC0= -25.57068 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909292976 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 286512741 +##$YMIN_p= -73654 +##END= diff --git a/Extracellular/DD/DD_Stage1/114/pdata/1/title b/Extracellular/DD/DD_Stage1/114/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dad92eb830ce9a23fdd2b80df16106355f9761bb --- /dev/null +++ b/Extracellular/DD/DD_Stage1/114/pdata/1/title @@ -0,0 +1 @@ +114, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1/114/pulseprogram b/Extracellular/DD/DD_Stage1/114/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/114/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1/115/acqu b/Extracellular/DD/DD_Stage1/115/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ 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+##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1/115/pdata/1/procs b/Extracellular/DD/DD_Stage1/115/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..8c055e8e86ff48e724ef8904a4678349639f5d97 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/115/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83955 +##$PC= 1 +##$PHC0= -26.0376 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909344788 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 284198287 +##$YMIN_p= -62908 +##END= diff --git a/Extracellular/DD/DD_Stage1/115/pdata/1/title b/Extracellular/DD/DD_Stage1/115/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..fc35a6986ae5c0305c9c1cbf53d1a35e9468a318 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/115/pdata/1/title @@ -0,0 +1 @@ +115, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1/115/pulseprogram b/Extracellular/DD/DD_Stage1/115/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/115/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1/116/acqu b/Extracellular/DD/DD_Stage1/116/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ 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+##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1/116/pdata/1/procs b/Extracellular/DD/DD_Stage1/116/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..31572653a4af6efa7ed3ebdc925e6ee22e880eb4 --- /dev/null +++ b/Extracellular/DD/DD_Stage1/116/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83965 +##$PC= 1 +##$PHC0= -25.20264 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909278976 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 266599473 +##$YMIN_p= -109702 +##END= diff --git a/Extracellular/DD/DD_Stage1/116/pdata/1/title b/Extracellular/DD/DD_Stage1/116/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..79d398e7923dadea9760e9bc8e71c30db0ce0cbf --- /dev/null +++ b/Extracellular/DD/DD_Stage1/116/pdata/1/title @@ -0,0 +1 @@ +116, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1/116/pulseprogram b/Extracellular/DD/DD_Stage1/116/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1/116/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/.DS_Store b/Extracellular/DD/DD_Stage1_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..b2987b877c133ca8c369939b0e42c76c7c3d6aff Binary files /dev/null and b/Extracellular/DD/DD_Stage1_CellFreeControl/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/131/acqu b/Extracellular/DD/DD_Stage1_CellFreeControl/131/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/131/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 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+##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/131/pdata/1/procs b/Extracellular/DD/DD_Stage1_CellFreeControl/131/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..418ce357dca7d9b5a1d1ded93911b7ba4c8d692e --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/131/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values 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0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83993 +##$PC= 1 +##$PHC0= -24.78516 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909078728 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 319343453 +##$YMIN_p= -70346 +##END= diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/131/pdata/1/title b/Extracellular/DD/DD_Stage1_CellFreeControl/131/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..5624c45b219aff8a9745c7bcad74ce6f4cf66986 --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/131/pdata/1/title @@ -0,0 +1 @@ +131, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/131/pulseprogram b/Extracellular/DD/DD_Stage1_CellFreeControl/131/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/131/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/132/acqu b/Extracellular/DD/DD_Stage1_CellFreeControl/132/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/132/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 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0000000000000000000000000000000000000000..8f30baa9419a23da43aba5e9ba69a9ad7297ddc9 --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/132/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 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0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 342449549 +##$YMIN_p= -98051 +##END= diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/132/pdata/1/title b/Extracellular/DD/DD_Stage1_CellFreeControl/132/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..a86ca07d91f326bd4021474c0fb80fe5ed1981e1 --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/132/pdata/1/title @@ -0,0 +1 @@ +132, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/132/pulseprogram b/Extracellular/DD/DD_Stage1_CellFreeControl/132/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/132/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/133/acqu b/Extracellular/DD/DD_Stage1_CellFreeControl/133/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/133/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 +##$DE= 55 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 12 +##$DQDMODE= 0 +##$DR= 22 +##$DS= 4 +##$DSPFIRM= 4 +##$DSPFVS= 0 +##$DTYPA= 0 +##$EXP= +##$FCUCHAN= (0..9) +0 2 0 0 0 0 0 0 0 0 +##$FL1= 90 +##$FL2= 90 +##$FL3= 90 +##$FL4= 90 +##$FN_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$FOV= 20 +##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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4200 +##$MASRLST= +##$MULEXPNO= (0..15) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$NBL= 1 +##$NC= 0 +##$NLOGCH= 2 +##$NOVFLW= 0 +##$NS= 32 +##$NUC1= <1H> +##$NUC2= +##$NUC3= +##$NUC4= +##$NUC5= +##$NUC6= +##$NUC7= +##$NUC8= +##$NUCLEUS= +##$NUSLIST= +##$NusAMOUNT= 25 +##$NusFPNZ= no +##$NusJSP= 0 +##$NusSEED= 54321 +##$NusSPTYPE= 0 +##$NusT2= 1 +##$NusTD= 0 +##$O1= 3296.2 +##$O2= 3297.086 +##$O3= 3297.086 +##$O4= 3297.086 +##$O5= 3297.086 +##$O6= 3297.086 +##$O7= 3297.086 +##$O8= 3297.086 +##$OVERFLW= 0 +##$P= (0..63) +21.06 21.06 42.12 0 0 16.5 25 50 20000 0 0 80000 80000 1000 0 0 1000 2500 +100000 600 0 0 0 0 0 72 100000 21.06 0 1000 0 0 20000 0 0 0 0 0 0 0 2000 +0 0 0 171 0 80000 46600 10000 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PACOIL= (0..15) +1 4 0 0 2 3 0 0 0 0 0 0 0 0 0 0 +##$PAPS= 2 +##$PARMODE= 0 +##$PCPD= (0..9) +100 65 80 100 100 100 100 100 100 100 +##$PEXSEL= (0..9) +1 1 1 1 1 1 1 1 1 1 +##$PHCOR= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PHLIST= 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a/Extracellular/DD/DD_Stage1_CellFreeControl/133/fid b/Extracellular/DD/DD_Stage1_CellFreeControl/133/fid new file mode 100644 index 0000000000000000000000000000000000000000..6a3da69a5824d0af255e75f3db18956a03f371cf Binary files /dev/null and b/Extracellular/DD/DD_Stage1_CellFreeControl/133/fid differ diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/1r b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..bfc60492618734cacad976d5e9a4c3c9d6eb07b3 Binary files /dev/null and b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/proc b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/procs b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..68fa2b86df5bd7bdaf04d4a8d813d6231da7efd3 --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83968 +##$PC= 1 +##$PHC0= -25.68054 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909255867 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 604308787 +##$YMIN_p= -106514 +##END= diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/title b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..a39180e021568e188f73ddd2b00be62f0c34b99d --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pdata/1/title @@ -0,0 +1 @@ +133, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage1_CellFreeControl/133/pulseprogram b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage1_CellFreeControl/133/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2/.DS_Store b/Extracellular/DD/DD_Stage2/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..26e12b48355b22766e4603ca2710d36a8f50e973 Binary files /dev/null and b/Extracellular/DD/DD_Stage2/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage2/211/acqu b/Extracellular/DD/DD_Stage2/211/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2/211/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 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+##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GRDPROG= <> +##$GRPDLY= -1 +##$HDDUTY= 20 +##$HDRATE= 1 +##$HGAIN= (0..3) +0 0 0 0 +##$HL1= 1 +##$HL2= 35 +##$HL3= 16 +##$HL4= 17 +##$HOLDER= 304 +##$HPMOD= (0..7) +0 0 0 0 0 0 0 0 +##$HPPRGN= 0 +##$IN= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$INF= (0..7) +0 0 0 0 0 0 0 0 +##$INP= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 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+##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/211/acqus b/Extracellular/DD/DD_Stage2/211/acqus new file mode 100644 index 0000000000000000000000000000000000000000..ff701aeaf7c2200a441ff9387955e2b507791600 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/211/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 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+##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84005 +##$PC= 1 +##$PHC0= -25.44434 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908998207 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 296363602 +##$YMIN_p= -51642 +##END= diff --git a/Extracellular/DD/DD_Stage2/211/pdata/1/title b/Extracellular/DD/DD_Stage2/211/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dde384fed5bcdf71a8a6c0d5d2c903201ca59394 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/211/pdata/1/title @@ -0,0 +1 @@ +211, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2/211/pulseprogram b/Extracellular/DD/DD_Stage2/211/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2/211/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2/212/acqu b/Extracellular/DD/DD_Stage2/212/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2/212/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/212/acqus b/Extracellular/DD/DD_Stage2/212/acqus new file mode 100644 index 0000000000000000000000000000000000000000..c88d00e17b964692e22816ae09f6ed17da3d8dea --- /dev/null +++ b/Extracellular/DD/DD_Stage2/212/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 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+##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2/212/pdata/1/procs b/Extracellular/DD/DD_Stage2/212/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..fa0ea4775dddd7af2ddb0be3f9db28dba7860eb0 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/212/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83978 +##$PC= 1 +##$PHC0= -25.5542 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909187248 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 528902928 +##$YMIN_p= -106866 +##END= diff --git a/Extracellular/DD/DD_Stage2/212/pdata/1/title b/Extracellular/DD/DD_Stage2/212/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..d57e6062da576d90327d97164f4e910788be1b3f --- /dev/null +++ b/Extracellular/DD/DD_Stage2/212/pdata/1/title @@ -0,0 +1 @@ +212, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2/212/pulseprogram b/Extracellular/DD/DD_Stage2/212/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2/212/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2/213/acqu b/Extracellular/DD/DD_Stage2/213/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2/213/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/213/acqus b/Extracellular/DD/DD_Stage2/213/acqus new file mode 100644 index 0000000000000000000000000000000000000000..b4d589f3a2348f591d4f63bebc29b3d24766372c --- /dev/null +++ b/Extracellular/DD/DD_Stage2/213/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 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+##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 23218620 +##$YMIN_a= -12359952 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/213/fid b/Extracellular/DD/DD_Stage2/213/fid new file mode 100644 index 0000000000000000000000000000000000000000..a444f15fc7fc327b88a6653f8ee0ac19720765a8 Binary files /dev/null and b/Extracellular/DD/DD_Stage2/213/fid differ diff --git a/Extracellular/DD/DD_Stage2/213/pdata/1/1r b/Extracellular/DD/DD_Stage2/213/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..a5e2660944882a970e91b309111ae2d54cda7e44 Binary files /dev/null and b/Extracellular/DD/DD_Stage2/213/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage2/213/pdata/1/proc b/Extracellular/DD/DD_Stage2/213/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/213/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2/213/pdata/1/procs b/Extracellular/DD/DD_Stage2/213/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..3e447433fe8483c982bd730045aa5bb9acc3deb1 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/213/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83986 +##$PC= 1 +##$PHC0= -25.66956 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909129837 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 295755976 +##$YMIN_p= -63791 +##END= diff --git a/Extracellular/DD/DD_Stage2/213/pdata/1/title b/Extracellular/DD/DD_Stage2/213/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..9adb31df24521269fd4cc097cc02beeaee2896c5 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/213/pdata/1/title @@ -0,0 +1 @@ +213, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2/213/pulseprogram b/Extracellular/DD/DD_Stage2/213/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2/213/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2/214/acqu b/Extracellular/DD/DD_Stage2/214/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2/214/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 24017966 +##$YMIN_a= -12491466 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/214/fid b/Extracellular/DD/DD_Stage2/214/fid new file mode 100644 index 0000000000000000000000000000000000000000..910b39e6074e1230a0f26748f2ea084e3be65ef2 Binary files /dev/null and b/Extracellular/DD/DD_Stage2/214/fid differ diff --git a/Extracellular/DD/DD_Stage2/214/pdata/1/1r b/Extracellular/DD/DD_Stage2/214/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..c1fcfdafa62a533ea4ce60b74a06d93eb03d65b0 Binary files /dev/null and b/Extracellular/DD/DD_Stage2/214/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage2/214/pdata/1/proc b/Extracellular/DD/DD_Stage2/214/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/214/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2/214/pdata/1/procs b/Extracellular/DD/DD_Stage2/214/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..00eb8f2c1d89d63db4e9c3d658b1442b8949dcde --- /dev/null +++ b/Extracellular/DD/DD_Stage2/214/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83981 +##$PC= 1 +##$PHC0= -25.18616 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909164146 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 293737080 +##$YMIN_p= -67013 +##END= diff --git a/Extracellular/DD/DD_Stage2/214/pdata/1/title b/Extracellular/DD/DD_Stage2/214/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..49c128f2006492f85565648ac8be76efe8a65243 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/214/pdata/1/title @@ -0,0 +1 @@ +214, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2/214/pulseprogram b/Extracellular/DD/DD_Stage2/214/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2/214/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2/215/acqu b/Extracellular/DD/DD_Stage2/215/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2/215/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0646e-05 9.176e-06 0 0 0.0071712 2.487e-05 0 2.487e-07 0 0.0071712 +0.0071712 0 0 0 0 0 0 0 1.464718e-05 2.276856e-05 1.06313e-05 5.733374e-05 +0 0 0 0 0 0 0.094997 5.4433 0 0 0 0.00010032 9.176e-06 0.00058726 0 0 0 +0 2.487e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.2003 +##$TE1= 300.2003 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 21706913 +##$YMIN_a= -11428559 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/215/fid b/Extracellular/DD/DD_Stage2/215/fid new file mode 100644 index 0000000000000000000000000000000000000000..956eea871c66b74cb9e85a9b3a92c4a071a347da Binary files /dev/null and b/Extracellular/DD/DD_Stage2/215/fid differ diff --git a/Extracellular/DD/DD_Stage2/215/pdata/1/1r b/Extracellular/DD/DD_Stage2/215/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..4df9c2f231d70ff5881485e61aac0240c7e2729d Binary files /dev/null and b/Extracellular/DD/DD_Stage2/215/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage2/215/pdata/1/proc b/Extracellular/DD/DD_Stage2/215/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/215/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2/215/pdata/1/procs b/Extracellular/DD/DD_Stage2/215/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..96889344c9d271fbe51ced6a213c2076a3ac28a9 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/215/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83957 +##$PC= 1 +##$PHC0= -25.20813 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909328682 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 532735909 +##$YMIN_p= -119106 +##END= diff --git a/Extracellular/DD/DD_Stage2/215/pdata/1/title b/Extracellular/DD/DD_Stage2/215/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..a041433841aa1f2e3d71ca23dd4329bb4903c925 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/215/pdata/1/title @@ -0,0 +1 @@ +215, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2/215/pulseprogram b/Extracellular/DD/DD_Stage2/215/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2/215/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2/216/acqu 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1.46962e-05 2.284476e-05 1.066688e-05 5.752562e-05 +0 0 0 0 0 0 0.095315 5.4616 0 0 0 0.00010065 9.2067e-06 0.00058923 0 0 +0 0 2.4953e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1898 +##$TE1= 300.1898 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22280816 +##$YMIN_a= -11862868 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2/216/fid b/Extracellular/DD/DD_Stage2/216/fid new file mode 100644 index 0000000000000000000000000000000000000000..c58129e20a78eee0d01564da5b29722c8066dcde Binary files /dev/null and b/Extracellular/DD/DD_Stage2/216/fid differ diff --git a/Extracellular/DD/DD_Stage2/216/pdata/1/1r b/Extracellular/DD/DD_Stage2/216/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..9759a98b75cf850c225f46c3f23a88549a5cd72f Binary files /dev/null and b/Extracellular/DD/DD_Stage2/216/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage2/216/pdata/1/proc b/Extracellular/DD/DD_Stage2/216/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/216/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2/216/pdata/1/procs b/Extracellular/DD/DD_Stage2/216/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..49497f7d4387a152a415ed051ce638beebbbedd9 --- /dev/null +++ b/Extracellular/DD/DD_Stage2/216/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83969 +##$PC= 1 +##$PHC0= -25.62012 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909243965 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 275517088 +##$YMIN_p= -64631 +##END= diff --git a/Extracellular/DD/DD_Stage2/216/pdata/1/title b/Extracellular/DD/DD_Stage2/216/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..04fa7dcf5442c6d0e8a6392a6d0904467ebe7aac --- /dev/null +++ b/Extracellular/DD/DD_Stage2/216/pdata/1/title @@ -0,0 +1 @@ +216, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2/216/pulseprogram b/Extracellular/DD/DD_Stage2/216/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2/216/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/.DS_Store b/Extracellular/DD/DD_Stage2_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..755f46bd2fcabfb21df98e6d271f9f12dceb26a1 Binary files /dev/null and b/Extracellular/DD/DD_Stage2_CellFreeControl/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/acqu b/Extracellular/DD/DD_Stage2_CellFreeControl/231/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/231/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> 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0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22859420 +##$YMIN_a= -12585552 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/fid b/Extracellular/DD/DD_Stage2_CellFreeControl/231/fid new file mode 100644 index 0000000000000000000000000000000000000000..bbe8c6127abadee1318a4da662cf8506771d5943 Binary files /dev/null and b/Extracellular/DD/DD_Stage2_CellFreeControl/231/fid differ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/1r b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..a9ab5154c31b573c0638af6627ba76305b69876b Binary files /dev/null and b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/proc b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/procs b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..34df8ceed00cc871e04f777a943cd37bbbd62b42 --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83979 +##$PC= 1 +##$PHC0= -25.01587 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909178146 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 297042781 +##$YMIN_p= -88565 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/title b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..1c7813859b525917a1bd7a38833e86c2b2ac6eab --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pdata/1/title @@ -0,0 +1 @@ +231, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/231/pulseprogram b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/231/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/acqu b/Extracellular/DD/DD_Stage2_CellFreeControl/232/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/232/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 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+##$TE= 300.1992 +##$TE1= 300.1992 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 26569688 +##$YMIN_a= -13855682 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/fid b/Extracellular/DD/DD_Stage2_CellFreeControl/232/fid new file mode 100644 index 0000000000000000000000000000000000000000..945d4277e79b17ac9dfdb2e91b7a8df5c3b7b233 Binary files /dev/null and b/Extracellular/DD/DD_Stage2_CellFreeControl/232/fid differ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/1r b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..c6c520cbc08c018ba269b9bc56e5975a3cb1c17c Binary files /dev/null and b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/proc b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/procs b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..215f96a8eab7c2c41e7be65a7e83237447a1735a --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83956 +##$PC= 1 +##$PHC0= -25.37292 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909337784 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 334497082 +##$YMIN_p= -87781 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/title b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..75c82abbab94fdb33eece7c9755cf7429a195847 --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pdata/1/title @@ -0,0 +1 @@ +232, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/232/pulseprogram b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/232/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/233/acqu b/Extracellular/DD/DD_Stage2_CellFreeControl/233/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/233/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 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0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/procs b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..89609819b80f14943e3fdfa6d213b2b5d7d3ed77 --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83961 +##$PC= 1 +##$PHC0= -25.78491 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909302078 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 298155309 +##$YMIN_p= -71894 +##END= diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/title b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..13dc771b26d35f7c61d939a39d73e2428d754a3a --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pdata/1/title @@ -0,0 +1 @@ +233, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage2_CellFreeControl/233/pulseprogram b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage2_CellFreeControl/233/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3/.DS_Store b/Extracellular/DD/DD_Stage3/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..43f3b9b185deded156b2c6983e108dec0f877c2f Binary files /dev/null and b/Extracellular/DD/DD_Stage3/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage3/311/acqu b/Extracellular/DD/DD_Stage3/311/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/311/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 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+##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage3/311/pdata/1/procs b/Extracellular/DD/DD_Stage3/311/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..96efc94029864ed120df60be70a46495c3f74b1e --- /dev/null +++ b/Extracellular/DD/DD_Stage3/311/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +w##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84052 +##$PC= 1 +##$PHC0= -25.26306 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908663521 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 357131881 +##$YMIN_p= -100068 +##END= diff --git a/Extracellular/DD/DD_Stage3/311/pdata/1/title b/Extracellular/DD/DD_Stage3/311/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f92e698bd965ef445dd09f9fdbe2dcad9a619f20 --- /dev/null +++ b/Extracellular/DD/DD_Stage3/311/pdata/1/title @@ -0,0 +1 @@ +311, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3/311/pulseprogram b/Extracellular/DD/DD_Stage3/311/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3/311/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3/312/acqu b/Extracellular/DD/DD_Stage3/312/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/312/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 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0000000000000000000000000000000000000000..14923393f2856e89eb759ba03f46c364b6220fce Binary files /dev/null and b/Extracellular/DD/DD_Stage3/312/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage3/312/pdata/1/proc b/Extracellular/DD/DD_Stage3/312/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage3/312/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 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+##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage3/312/pdata/1/procs b/Extracellular/DD/DD_Stage3/312/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..ac60f4ea56987a5996f6edf31b18fcecf4589c8a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/312/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84042 +##$PC= 1 +##$PHC0= -25.88379 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990873494 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 331639950 +##$YMIN_p= -82633 +##END= diff --git a/Extracellular/DD/DD_Stage3/312/pdata/1/title b/Extracellular/DD/DD_Stage3/312/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dbfdceddcd0cadca489488952fa0366cbb9fcc10 --- /dev/null +++ b/Extracellular/DD/DD_Stage3/312/pdata/1/title @@ -0,0 +1 @@ +312, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3/312/pulseprogram b/Extracellular/DD/DD_Stage3/312/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3/312/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3/313/acqu b/Extracellular/DD/DD_Stage3/313/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/313/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 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+##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84025 +##$PC= 1 +##$PHC0= -25.61462 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908856773 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 400796143 +##$YMIN_p= -110876 +##END= diff --git a/Extracellular/DD/DD_Stage3/313/pdata/1/title b/Extracellular/DD/DD_Stage3/313/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f558e2e3ef5f9315bd1d8682c2085c4be782ce10 --- /dev/null +++ b/Extracellular/DD/DD_Stage3/313/pdata/1/title @@ -0,0 +1 @@ +313, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3/313/pulseprogram b/Extracellular/DD/DD_Stage3/313/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3/313/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3/314/acqu b/Extracellular/DD/DD_Stage3/314/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/314/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84058 +##$PC= 1 +##$PHC0= -26.07056 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908625717 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 499946001 +##$YMIN_p= -141607 +##END= diff --git a/Extracellular/DD/DD_Stage3/314/pdata/1/title b/Extracellular/DD/DD_Stage3/314/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..e4a1245eb7857a83a46abf8c2e5986c0c9aab79e --- /dev/null +++ b/Extracellular/DD/DD_Stage3/314/pdata/1/title @@ -0,0 +1 @@ +314, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3/314/pulseprogram b/Extracellular/DD/DD_Stage3/314/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3/314/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3/315/acqu b/Extracellular/DD/DD_Stage3/315/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/315/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84044 +##$PC= 1 +##$PHC0= -25.36194 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990872094 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 268955594 +##$YMIN_p= -78427 +##END= diff --git a/Extracellular/DD/DD_Stage3/315/pdata/1/title b/Extracellular/DD/DD_Stage3/315/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..824e099d68bf9e3bbc4c75c1068249936ad99998 --- /dev/null +++ b/Extracellular/DD/DD_Stage3/315/pdata/1/title @@ -0,0 +1 @@ +315, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3/315/pulseprogram b/Extracellular/DD/DD_Stage3/315/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3/315/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3/316/acqu b/Extracellular/DD/DD_Stage3/316/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3/316/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage3/316/pdata/1/procs b/Extracellular/DD/DD_Stage3/316/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..85e6efd0bdbf847a95f33d754977bf5c5d2961f7 --- /dev/null +++ b/Extracellular/DD/DD_Stage3/316/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84045 +##$PC= 1 +##$PHC0= -25.65857 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908717438 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 278295554 +##$YMIN_p= -55583 +##END= diff --git a/Extracellular/DD/DD_Stage3/316/pdata/1/title b/Extracellular/DD/DD_Stage3/316/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..157c32cb811c776e3eef5899d6add588ce36cceb --- /dev/null +++ b/Extracellular/DD/DD_Stage3/316/pdata/1/title @@ -0,0 +1 @@ +316, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3/316/pulseprogram b/Extracellular/DD/DD_Stage3/316/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3/316/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/.DS_Store b/Extracellular/DD/DD_Stage3_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..dcc2e3908d817f96c024badbbec66cbd9aec3827 Binary files /dev/null and b/Extracellular/DD/DD_Stage3_CellFreeControl/.DS_Store differ diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/331/acqu b/Extracellular/DD/DD_Stage3_CellFreeControl/331/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/331/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) 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b/Extracellular/DD/DD_Stage3_CellFreeControl/331/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..a19f208d1daaa9972e3deed280fb1bafba84591f --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/331/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84071 +##$PC= 1 +##$PHC0= -25.7135 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908531891 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 311472159 +##$YMIN_p= -79619 +##END= diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/331/pdata/1/title b/Extracellular/DD/DD_Stage3_CellFreeControl/331/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f4f63af210e5d4271c6a90bbdd226e0c93a81998 --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/331/pdata/1/title @@ -0,0 +1 @@ +331, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/331/pulseprogram b/Extracellular/DD/DD_Stage3_CellFreeControl/331/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/331/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/332/acqu b/Extracellular/DD/DD_Stage3_CellFreeControl/332/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/332/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 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<1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/332/pdata/1/procs b/Extracellular/DD/DD_Stage3_CellFreeControl/332/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..3c8159b658eb084890095672f99435aec9a5e524 --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/332/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 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+##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84055 +##$PC= 1 +##$PHC0= -26.06506 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908643921 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 271362921 +##$YMIN_p= -75667 +##END= diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/332/pdata/1/title b/Extracellular/DD/DD_Stage3_CellFreeControl/332/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..c5154ef8de832969ed8bb0377ae6cccbd291fe64 --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/332/pdata/1/title @@ -0,0 +1 @@ +332, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/332/pulseprogram b/Extracellular/DD/DD_Stage3_CellFreeControl/332/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/332/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/333/acqu b/Extracellular/DD/DD_Stage3_CellFreeControl/333/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/333/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 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Binary files /dev/null and b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/1r differ diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/proc b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 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+##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/procs b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..9c8105fcd7bab1daf91fcca98f09b46438a12dfa --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84041 +##$PC= 1 +##$PHC0= -25.10925 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990874334 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 278578357 +##$YMIN_p= -70804 +##END= diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/title b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..6dcb42db70113bf50caf23e0e28e8255fd8b9e8e --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pdata/1/title @@ -0,0 +1 @@ +333, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DD/DD_Stage3_CellFreeControl/333/pulseprogram b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DD/DD_Stage3_CellFreeControl/333/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/.DS_Store b/Extracellular/DDvsSD/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..ecae93a4f8e9dcfae798a17470f77f3360d75001 Binary files /dev/null and b/Extracellular/DDvsSD/.DS_Store differ diff --git a/Extracellular/DDvsSD/DD_Stage1/.DS_Store b/Extracellular/DDvsSD/DD_Stage1/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..d6716c2d5fa9036a3fb307a89e2c0f437545730d Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/.DS_Store differ diff --git a/Extracellular/DDvsSD/DD_Stage1/111/.DS_Store b/Extracellular/DDvsSD/DD_Stage1/111/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..e4e223b4404c1bb012290cbac7fade36b42a05f8 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/111/.DS_Store differ diff --git a/Extracellular/DDvsSD/DD_Stage1/111/acqu b/Extracellular/DDvsSD/DD_Stage1/111/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/111/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 +##$DE= 55 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 12 +##$DQDMODE= 0 +##$DR= 22 +##$DS= 4 +##$DSPFIRM= 4 +##$DSPFVS= 0 +##$DTYPA= 0 +##$EXP= +##$FCUCHAN= (0..9) +0 2 0 0 0 0 0 0 0 0 +##$FL1= 90 +##$FL2= 90 +##$FL3= 90 +##$FL4= 90 +##$FN_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$FOV= 20 +##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GRDPROG= <> +##$GRPDLY= -1 +##$HDDUTY= 20 +##$HDRATE= 1 +##$HGAIN= (0..3) +0 0 0 0 +##$HL1= 1 +##$HL2= 35 +##$HL3= 16 +##$HL4= 17 +##$HOLDER= 304 +##$HPMOD= (0..7) +0 0 0 0 0 0 0 0 +##$HPPRGN= 0 +##$IN= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$INF= (0..7) +0 0 0 0 0 0 0 0 +##$INP= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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+##$O8= 3297.086 +##$OVERFLW= 0 +##$P= (0..63) +21.06 21.06 42.12 0 0 16.5 25 50 20000 0 0 80000 80000 1000 0 0 1000 2500 +100000 600 0 0 0 0 0 72 100000 21.06 0 1000 0 0 20000 0 0 0 0 0 0 0 2000 +0 0 0 171 0 80000 46600 10000 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PACOIL= (0..15) +1 4 0 0 2 3 0 0 0 0 0 0 0 0 0 0 +##$PAPS= 2 +##$PARMODE= 0 +##$PCPD= (0..9) +100 65 80 100 100 100 100 100 100 100 +##$PEXSEL= (0..9) +1 1 1 1 1 1 1 1 1 1 +##$PHCOR= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PHLIST= <> +##$PHP= 1 +##$PH_ref= 0 +##$PL= (0..63) +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 +##$PLSTEP= 0.1 +##$PLSTRT= -6 +##$PLW= (0..63) +0 5.7 0 0 0 0 0 0 0 2.528085e-05 4.0465 0.39516 0 0 0 0 0 0 5.7 0.59859 +0 0 0 0 0 0 0 1.9514 0 4.0465 0 0 4.0465e-06 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120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 +##$SPECTR= 0 +##$SPINCNT= 0 +##$SPNAM= (0..63) +<> <> + <> <> <> + <> <> + <> <> <> <> <> <> +<> <> <> <> <> <> +<> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> +##$SPOAL= (0..63) +0.5 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +1 1 1 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 +##$SPOFFS= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPPEX= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0995e-05 9.3311e-06 0 0 0.0072924 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<> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/111/acqus b/Extracellular/DDvsSD/DD_Stage1/111/acqus new file mode 100644 index 0000000000000000000000000000000000000000..4c1879cf5f0228bb48810928f629e87a6afebf01 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/111/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 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+##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/111/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage1/111/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..76a6909489b5e4eca1cce0ab655495f101279e7f --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/111/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83982 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909158546 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 281892851 +##$YMIN_p= -70187 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/111/pdata/1/title b/Extracellular/DDvsSD/DD_Stage1/111/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..fe75f2d6fdca3819d88b6894c0a0096b2ec525cc --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/111/pdata/1/title @@ -0,0 +1 @@ +111, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage1/111/pulseprogram b/Extracellular/DDvsSD/DD_Stage1/111/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/111/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage1/112/.DS_Store b/Extracellular/DDvsSD/DD_Stage1/112/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..8aca75a32ae599da59f47fbf45fafe551b115189 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/112/.DS_Store differ diff --git a/Extracellular/DDvsSD/DD_Stage1/112/acqu b/Extracellular/DDvsSD/DD_Stage1/112/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/112/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 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a/Extracellular/DDvsSD/DD_Stage1/112/acqus b/Extracellular/DDvsSD/DD_Stage1/112/acqus new file mode 100644 index 0000000000000000000000000000000000000000..fc2123871d79c8fdf68ecf58afd9a1e443f55b49 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/112/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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+##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/112/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage1/112/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..22c0dae8a84943788b04615af9aa7ecac4f6c9db --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/112/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83977 +##$PC= 1 +##$PHC0= -25.34546 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990919355 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 275792005 +##$YMIN_p= -66786 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/112/pdata/1/title b/Extracellular/DDvsSD/DD_Stage1/112/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..860a5676a63df2115ce98aee9ddd2ca50c2c0885 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/112/pdata/1/title @@ -0,0 +1 @@ +112, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage1/112/pulseprogram b/Extracellular/DDvsSD/DD_Stage1/112/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/112/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage1/113/acqu b/Extracellular/DDvsSD/DD_Stage1/113/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/113/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 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(0..7) +0 0 0 0 0 0 0 0 +##$FOV= 20 +##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GRDPROG= <> +##$GRPDLY= -1 +##$HDDUTY= 20 +##$HDRATE= 1 +##$HGAIN= (0..3) +0 0 0 0 +##$HL1= 1 +##$HL2= 35 +##$HL3= 16 +##$HL4= 17 +##$HOLDER= 304 +##$HPMOD= (0..7) +0 0 0 0 0 0 0 0 +##$HPPRGN= 0 +##$IN= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$INF= (0..7) +0 0 0 0 0 0 0 0 +##$INP= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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0 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/113/acqus b/Extracellular/DDvsSD/DD_Stage1/113/acqus new file mode 100644 index 0000000000000000000000000000000000000000..f021cad348ee1ec94af4bb4970ec39dd91983b77 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/113/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..20932627abc7db287c4c505f1bbf187aefcf2c5b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8396 +##$PC= 1 +##$PHC0= -25.75745 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990931398 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 323053322 +##$YMIN_p= -76587 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/title b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..3e9b72a293cadcbd8fc7d3fb16ba6128dfc98b1c --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/113/pdata/1/title @@ -0,0 +1 @@ +113, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage1/113/pulseprogram b/Extracellular/DDvsSD/DD_Stage1/113/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/113/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage1/114/acqu b/Extracellular/DDvsSD/DD_Stage1/114/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/114/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 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120 120 120 +##$PLSTEP= 0.1 +##$PLSTRT= -6 +##$PLW= (0..63) +0 5.7 0 0 0 0 0 0 0 2.499357e-05 3.9978 0.39041 0 0 0 0 0 0 5.7 0.59138 +0 0 0 0 0 0 0 1.9279 0 3.9978 0 0 3.9978e-06 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PLWMAX= (0..7) +63.6 0 0 0 0 0 0 0 +##$PQPHASE= 0 +##$PQSCALE= 1 +##$PR= 1 +##$PRECHAN= (0..15) +-1 4 0 1 5 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$PRGAIN= 0 +##$PROBHD= +##$PULPROG= +##$PW= 0 +##$PYNM= +##$ProjAngle= 0 +##$QNP= 1 +##$RD= 0 +##$RECCHAN= (0..15) +0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECPH= 0 +##$RECPRE= (0..15) +-1 0 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$RECPRFX= (0..15) +1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECSEL= (0..15) +0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RG= 56.72 +##$RO= 0 +##$RSEL= (0..15) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$S= (0..7) +83 4 83 83 83 83 83 83 +##$SELREC= (0..9) +0 0 0 0 0 0 0 0 0 0 +##$SFO1= 700.1732962 +##$SFO2= 700.173297086 +##$SFO3= 700.173297086 +##$SFO4= 700.173297086 +##$SFO5= 700.173297086 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0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0742e-05 9.2188e-06 0 0 0.0072046 2.4986e-05 0 2.4986e-07 0 0.0072046 +0.0072046 0 0 0 0 0 0 0 1.47158e-05 2.287524e-05 1.068112e-05 5.760238e-05 +0 0 0 0 0 0 0.095439 5.4687 0 0 0 0.00010078 9.2188e-06 0.00059 0 0 0 0 +2.4986e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.2003 +##$TE1= 300.2003 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22158665 +##$YMIN_a= -11927450 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/114/fid b/Extracellular/DDvsSD/DD_Stage1/114/fid new file mode 100644 index 0000000000000000000000000000000000000000..644739891ad94da4607d3cb596bf6aa0d4c3a5be Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/114/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..c07f94d69d1d13f7764aafb54f49b23fb8ed3454 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..0115da01d4eb70d12a8325e0ae4c9fddfc4b0c33 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83963 +##$PC= 1 +##$PHC0= -25.57068 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909292976 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 286512741 +##$YMIN_p= -73654 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/title b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dad92eb830ce9a23fdd2b80df16106355f9761bb --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/114/pdata/1/title @@ -0,0 +1 @@ +114, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage1/114/pulseprogram b/Extracellular/DDvsSD/DD_Stage1/114/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/114/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage1/115/acqu b/Extracellular/DDvsSD/DD_Stage1/115/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/115/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 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0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0773e-05 9.2323e-06 0 0 0.0072152 2.5023e-05 0 2.5023e-07 0 0.0072152 +0.0072152 0 0 0 0 0 0 0 1.473705e-05 2.290826e-05 1.069653e-05 5.768552e-05 +0 0 0 0 0 0 0.095579 5.4767 0 0 0 0.00010093 9.2323e-06 0.00059087 0 0 +0 0 2.5023e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.2 +##$TE1= 300.2 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 23117190 +##$YMIN_a= -12691884 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/115/fid b/Extracellular/DDvsSD/DD_Stage1/115/fid new file mode 100644 index 0000000000000000000000000000000000000000..6ac28fc8e181067c97a60bd3298a073fd1d7864e Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/115/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..f2e6d54432e0eef2ff2fb16c17530022aa72a9f8 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..8c055e8e86ff48e724ef8904a4678349639f5d97 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83955 +##$PC= 1 +##$PHC0= -26.0376 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909344788 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 284198287 +##$YMIN_p= -62908 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/title b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..fc35a6986ae5c0305c9c1cbf53d1a35e9468a318 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/115/pdata/1/title @@ -0,0 +1 @@ +115, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage1/115/pulseprogram b/Extracellular/DDvsSD/DD_Stage1/115/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/115/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage1/116/acqu b/Extracellular/DDvsSD/DD_Stage1/116/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/116/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 +##$DE= 55 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 12 +##$DQDMODE= 0 +##$DR= 22 +##$DS= 4 +##$DSPFIRM= 4 +##$DSPFVS= 0 +##$DTYPA= 0 +##$EXP= +##$FCUCHAN= (0..9) +0 2 0 0 0 0 0 0 0 0 +##$FL1= 90 +##$FL2= 90 +##$FL3= 90 +##$FL4= 90 +##$FN_INDIRECT= 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0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0573e-05 9.1437e-06 0 0 0.007146 2.4782e-05 0 2.4782e-07 0 0.007146 +0.007146 0 0 0 0 0 0 0 1.45957e-05 2.268855e-05 1.059394e-05 5.713227e-05 +0 0 0 0 0 0 0.094662 5.4241 0 0 0 9.9963e-05 9.1437e-06 0.00058519 0 0 +0 0 2.4782e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.2019 +##$TE1= 300.2019 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 21641413 +##$YMIN_a= -11464399 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/116/fid b/Extracellular/DDvsSD/DD_Stage1/116/fid new file mode 100644 index 0000000000000000000000000000000000000000..730da038dc73555b70ce207178ac11f34f7a8515 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/116/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..05369a4d569deff1c450f3d0e64784992359c261 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..31572653a4af6efa7ed3ebdc925e6ee22e880eb4 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83965 +##$PC= 1 +##$PHC0= -25.20264 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909278976 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 266599473 +##$YMIN_p= -109702 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/title b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..79d398e7923dadea9760e9bc8e71c30db0ce0cbf --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/116/pdata/1/title @@ -0,0 +1 @@ +116, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage1/116/pulseprogram b/Extracellular/DDvsSD/DD_Stage1/116/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage1/116/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage2/.DS_Store b/Extracellular/DDvsSD/DD_Stage2/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..26e12b48355b22766e4603ca2710d36a8f50e973 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/.DS_Store differ diff --git a/Extracellular/DDvsSD/DD_Stage2/211/acqu b/Extracellular/DDvsSD/DD_Stage2/211/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/211/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 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300.1974 +##$TE1= 300.1974 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 23740088 +##$YMIN_a= -12492817 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/211/fid b/Extracellular/DDvsSD/DD_Stage2/211/fid new file mode 100644 index 0000000000000000000000000000000000000000..ba2d71176fdce7c84c57177a6acb4967b1bc2b83 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/211/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..3282104b641582aabae06bbeecb30ddce674f888 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..bc5fce56b5155eaafb968fb4167f6457f0abd9a4 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84005 +##$PC= 1 +##$PHC0= -25.44434 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908998207 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 296363602 +##$YMIN_p= -51642 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/title b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dde384fed5bcdf71a8a6c0d5d2c903201ca59394 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/211/pdata/1/title @@ -0,0 +1 @@ +211, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage2/211/pulseprogram b/Extracellular/DDvsSD/DD_Stage2/211/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/211/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage2/212/acqu b/Extracellular/DDvsSD/DD_Stage2/212/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/212/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH 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0000000000000000000000000000000000000000..361d4b221566221a5632f2f7b25c9c959d7fdbe7 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/212/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..1e4abb9190a518f3707060a9ca3b4c3a93210043 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..fa0ea4775dddd7af2ddb0be3f9db28dba7860eb0 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83978 +##$PC= 1 +##$PHC0= -25.5542 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909187248 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 528902928 +##$YMIN_p= -106866 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/title b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..d57e6062da576d90327d97164f4e910788be1b3f --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/212/pdata/1/title @@ -0,0 +1 @@ +212, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage2/212/pulseprogram b/Extracellular/DDvsSD/DD_Stage2/212/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/212/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage2/213/acqu b/Extracellular/DDvsSD/DD_Stage2/213/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/213/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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0000000000000000000000000000000000000000..a444f15fc7fc327b88a6653f8ee0ac19720765a8 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/213/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..a5e2660944882a970e91b309111ae2d54cda7e44 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..3e447433fe8483c982bd730045aa5bb9acc3deb1 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83986 +##$PC= 1 +##$PHC0= -25.66956 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909129837 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 295755976 +##$YMIN_p= -63791 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/title b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..9adb31df24521269fd4cc097cc02beeaee2896c5 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/213/pdata/1/title @@ -0,0 +1 @@ +213, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage2/213/pulseprogram b/Extracellular/DDvsSD/DD_Stage2/213/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/213/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage2/214/acqu b/Extracellular/DDvsSD/DD_Stage2/214/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/214/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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0000000000000000000000000000000000000000..910b39e6074e1230a0f26748f2ea084e3be65ef2 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/214/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..c1fcfdafa62a533ea4ce60b74a06d93eb03d65b0 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..00eb8f2c1d89d63db4e9c3d658b1442b8949dcde --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83981 +##$PC= 1 +##$PHC0= -25.18616 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909164146 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 293737080 +##$YMIN_p= -67013 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/title b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..49c128f2006492f85565648ac8be76efe8a65243 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/214/pdata/1/title @@ -0,0 +1 @@ +214, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage2/214/pulseprogram b/Extracellular/DDvsSD/DD_Stage2/214/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/214/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage2/215/acqu b/Extracellular/DDvsSD/DD_Stage2/215/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/215/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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0000000000000000000000000000000000000000..956eea871c66b74cb9e85a9b3a92c4a071a347da Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/215/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..4df9c2f231d70ff5881485e61aac0240c7e2729d Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..96889344c9d271fbe51ced6a213c2076a3ac28a9 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83957 +##$PC= 1 +##$PHC0= -25.20813 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909328682 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 532735909 +##$YMIN_p= -119106 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/title b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..a041433841aa1f2e3d71ca23dd4329bb4903c925 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/215/pdata/1/title @@ -0,0 +1 @@ +215, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage2/215/pulseprogram b/Extracellular/DDvsSD/DD_Stage2/215/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/215/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage2/216/acqu b/Extracellular/DDvsSD/DD_Stage2/216/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/216/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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+##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1898 +##$TE1= 300.1898 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22280816 +##$YMIN_a= -11862868 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/216/fid b/Extracellular/DDvsSD/DD_Stage2/216/fid new file mode 100644 index 0000000000000000000000000000000000000000..c58129e20a78eee0d01564da5b29722c8066dcde Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/216/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..9759a98b75cf850c225f46c3f23a88549a5cd72f Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..49497f7d4387a152a415ed051ce638beebbbedd9 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83969 +##$PC= 1 +##$PHC0= -25.62012 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909243965 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 275517088 +##$YMIN_p= -64631 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/title b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..04fa7dcf5442c6d0e8a6392a6d0904467ebe7aac --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/216/pdata/1/title @@ -0,0 +1 @@ +216, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage2/216/pulseprogram b/Extracellular/DDvsSD/DD_Stage2/216/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage2/216/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage3/.DS_Store b/Extracellular/DDvsSD/DD_Stage3/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..43f3b9b185deded156b2c6983e108dec0f877c2f Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/.DS_Store differ diff --git a/Extracellular/DDvsSD/DD_Stage3/311/acqu b/Extracellular/DDvsSD/DD_Stage3/311/acqu new file mode 100644 index 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5.755121e-05 +0 0 0 0 0 0 0.095354 5.4638 0 0 0 0.00010069 9.2105e-06 0.00058947 0 0 +0 0 2.4964e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1991 +##$TE1= 300.1991 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 28244796 +##$YMIN_a= -14508102 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/311/fid b/Extracellular/DDvsSD/DD_Stage3/311/fid new file mode 100644 index 0000000000000000000000000000000000000000..005f3f81769c8831629a5c56e83ebe429864a2c3 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/311/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..77fa15c5a71d4b1a6737e5458e18eb1668b92c3c Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..96efc94029864ed120df60be70a46495c3f74b1e --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +w##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84052 +##$PC= 1 +##$PHC0= -25.26306 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908663521 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 357131881 +##$YMIN_p= -100068 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/title b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f92e698bd965ef445dd09f9fdbe2dcad9a619f20 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/311/pdata/1/title @@ -0,0 +1 @@ +311, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage3/311/pulseprogram b/Extracellular/DDvsSD/DD_Stage3/311/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/311/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage3/312/acqu b/Extracellular/DDvsSD/DD_Stage3/312/acqu new file mode 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5.812365e-05 0 0 0 +0 0 0 0.096305 5.5183 0 0 0 0.0001017 9.3024e-06 0.00059535 0 0 0 0 2.5213e-07 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1997 +##$TE1= 300.1997 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 26803800 +##$YMIN_a= -14211641 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/312/fid b/Extracellular/DDvsSD/DD_Stage3/312/fid new file mode 100644 index 0000000000000000000000000000000000000000..2f7a721949b96b1127b73b1eaa5f1de7c65e2b61 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/312/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..14923393f2856e89eb759ba03f46c364b6220fce Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..ac60f4ea56987a5996f6edf31b18fcecf4589c8a --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84042 +##$PC= 1 +##$PHC0= -25.88379 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990873494 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 331639950 +##$YMIN_p= -82633 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/title b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dbfdceddcd0cadca489488952fa0366cbb9fcc10 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/312/pdata/1/title @@ -0,0 +1 @@ +312, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage3/312/pulseprogram b/Extracellular/DDvsSD/DD_Stage3/312/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/312/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage3/313/acqu b/Extracellular/DDvsSD/DD_Stage3/313/acqu new file mode 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5.799893e-05 +0 0 0 0 0 0 0.096099 5.5065 0 0 0 0.00010148 9.2825e-06 0.00059408 0 0 +0 0 2.5159e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1998 +##$TE1= 300.1998 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 19190364 +##$YMIN_a= -10347259 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/313/fid b/Extracellular/DDvsSD/DD_Stage3/313/fid new file mode 100644 index 0000000000000000000000000000000000000000..97706024ae50b6e0418f6b3dba8fba3d39c8e43b Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/313/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..57ebc2b38d6cb8a75eef172320eb62c2d8dc03c3 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..e500b1d3c03b5cccd150de7ef9ca376cf2ce489d --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84025 +##$PC= 1 +##$PHC0= -25.61462 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908856773 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 400796143 +##$YMIN_p= -110876 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/title b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f558e2e3ef5f9315bd1d8682c2085c4be782ce10 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/313/pdata/1/title @@ -0,0 +1 @@ +313, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage3/313/pulseprogram b/Extracellular/DDvsSD/DD_Stage3/313/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/313/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage3/314/acqu b/Extracellular/DDvsSD/DD_Stage3/314/acqu new file mode 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5.876005e-05 +0 0 0 0 0 0 0.097357 5.5786 0 0 0 0.00010281 9.404e-06 0.00060186 0 0 0 +0 2.5488e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.201 +##$TE1= 300.201 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 20943315 +##$YMIN_a= -11418839 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/314/fid b/Extracellular/DDvsSD/DD_Stage3/314/fid new file mode 100644 index 0000000000000000000000000000000000000000..c074423caf9265e7c2027fc1997bfd3c9ed01341 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/314/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..551fafa505e58411b0f8d57d5d0c1cc0fe5d456b Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..dac6630b45db0df614f41b95735bbe2100d4c1c0 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84058 +##$PC= 1 +##$PHC0= -26.07056 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908625717 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 499946001 +##$YMIN_p= -141607 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/title b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..e4a1245eb7857a83a46abf8c2e5986c0c9aab79e --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/314/pdata/1/title @@ -0,0 +1 @@ +314, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage3/314/pulseprogram b/Extracellular/DDvsSD/DD_Stage3/314/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/314/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage3/315/acqu b/Extracellular/DDvsSD/DD_Stage3/315/acqu new file mode 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5.785822e-05 +0 0 0 0 0 0 0.095864 5.493 0 0 0 0.00010123 9.2598e-06 0.00059263 0 0 0 +0 2.5097e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1996 +##$TE1= 300.1996 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22477770 +##$YMIN_a= -11808690 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/315/fid b/Extracellular/DDvsSD/DD_Stage3/315/fid new file mode 100644 index 0000000000000000000000000000000000000000..7394013bd0e52a0340d7cbf2d71879bb8d7b5f2c Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/315/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..9dd33a0b94d41643bac3fb142e5f292a14abdfdf Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..c2c7f30eaca37409c0429978f43f3ec174e25d3c --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84044 +##$PC= 1 +##$PHC0= -25.36194 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990872094 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 268955594 +##$YMIN_p= -78427 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/title b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..824e099d68bf9e3bbc4c75c1068249936ad99998 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/315/pdata/1/title @@ -0,0 +1 @@ +315, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage3/315/pulseprogram b/Extracellular/DDvsSD/DD_Stage3/315/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/315/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/DD_Stage3/316/acqu b/Extracellular/DDvsSD/DD_Stage3/316/acqu new file mode 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5.778146e-05 +0 0 0 0 0 0 0.095739 5.4858 0 0 0 0.0001011 9.2477e-06 0.00059185 0 0 0 +0 2.5064e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1988 +##$TE1= 300.1988 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 23065682 +##$YMIN_a= -12244644 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/316/fid b/Extracellular/DDvsSD/DD_Stage3/316/fid new file mode 100644 index 0000000000000000000000000000000000000000..6091bec434818de11f08587289cfdf3a25defb99 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/316/fid differ diff --git a/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/1r b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..7a52587536a5d05e55c1d201ad48cf17442ec9a7 Binary files /dev/null and b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/proc b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/procs b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..85e6efd0bdbf847a95f33d754977bf5c5d2961f7 --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84045 +##$PC= 1 +##$PHC0= -25.65857 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908717438 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 278295554 +##$YMIN_p= -55583 +##END= diff --git a/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/title b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..157c32cb811c776e3eef5899d6add588ce36cceb --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/316/pdata/1/title @@ -0,0 +1 @@ +316, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/DD_Stage3/316/pulseprogram b/Extracellular/DDvsSD/DD_Stage3/316/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/DD_Stage3/316/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage1/.DS_Store b/Extracellular/DDvsSD/SD_Stage1/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..8eddadee93588512dad978838c148165d8375ebf Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage1/.DS_Store differ diff --git a/Extracellular/DDvsSD/SD_Stage1/411/acqu b/Extracellular/DDvsSD/SD_Stage1/411/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/411/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 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0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 16231251 +##$YMIN_a= -8565247 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/411/fid b/Extracellular/DDvsSD/SD_Stage1/411/fid new file mode 100644 index 0000000000000000000000000000000000000000..853911173e0242270380c1898ebe81087ac20eb9 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage1/411/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..e87eb1b1138975c02c8f2c4072f3c168c350420a Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..5038b1eea54ad16c908208d934493065e8b702fb --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8398 +##$PC= 1 +##$PHC0= -24.81262 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909167648 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 313642930 +##$YMIN_p= -68872 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/title b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..27af325fb683373b43ff15680ab86810370aef18 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/411/pdata/1/title @@ -0,0 +1 @@ +411, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage1/411/pulseprogram b/Extracellular/DDvsSD/SD_Stage1/411/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/411/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage1/412/acqu b/Extracellular/DDvsSD/SD_Stage1/412/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/412/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 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a/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..30a06a0dae85843fee7485ac713519f75e114c38 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83948 +##$PC= 1 +##$PHC0= -25.7135 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909394501 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 272378567 +##$YMIN_p= -61077 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/title b/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..b732b1769fe8a766f7473667b4c4984212bf0e96 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/412/pdata/1/title @@ -0,0 +1 @@ +412, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage1/412/pulseprogram b/Extracellular/DDvsSD/SD_Stage1/412/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/412/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage1/413/acqu b/Extracellular/DDvsSD/SD_Stage1/413/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/413/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 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a/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..f2725bde1cc34236c2160aae01f6c789e94e46a1 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83958 +##$PC= 1 +##$PHC0= -25.10925 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909321686 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 515098398 +##$YMIN_p= -120903 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/title b/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..86defa883c35926b421e697829d8e477016b4dda --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/413/pdata/1/title @@ -0,0 +1 @@ +413, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage1/413/pulseprogram b/Extracellular/DDvsSD/SD_Stage1/413/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/413/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage1/414/acqu b/Extracellular/DDvsSD/SD_Stage1/414/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/414/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 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a/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..62434009287d30b5fc38608a709c04e2a155361e --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83935 +##$PC= 1 +##$PHC0= -25.3125 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909487625 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 269565943 +##$YMIN_p= -66570 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/title b/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..bedb36d25dff6bebe2031a0db2b30ff589cdd83a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/414/pdata/1/title @@ -0,0 +1 @@ +414, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage1/414/pulseprogram b/Extracellular/DDvsSD/SD_Stage1/414/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/414/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage1/415/acqu b/Extracellular/DDvsSD/SD_Stage1/415/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/415/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 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a/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..54db6f827ab2674da5e151e1bb90fbbd4085c07e --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83945 +##$PC= 1 +##$PHC0= -25.3894 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909416908 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 457661231 +##$YMIN_p= -105595 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/title b/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..756283c7a9cbe96ed7cf012f02b540ec0326495b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/415/pdata/1/title @@ -0,0 +1 @@ +415, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage1/415/pulseprogram b/Extracellular/DDvsSD/SD_Stage1/415/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/415/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage1/416/acqu b/Extracellular/DDvsSD/SD_Stage1/416/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/416/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 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a/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..839c4cb589e353e5203dffeac5d13ede9dda6afc --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83935 +##$PC= 1 +##$PHC0= -25.76294 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909486221 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 318126917 +##$YMIN_p= -89740 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/title b/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..643b476b3f17c24ef8d7b50b6f7f23acc72ee76a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/416/pdata/1/title @@ -0,0 +1 @@ +416, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage1/416/pulseprogram b/Extracellular/DDvsSD/SD_Stage1/416/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage1/416/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage2/.DS_Store b/Extracellular/DDvsSD/SD_Stage2/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..57077b97e701da3c4dd1127f008542ab527d3c3d Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/.DS_Store differ diff --git a/Extracellular/DDvsSD/SD_Stage2/511/acqu b/Extracellular/DDvsSD/SD_Stage2/511/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/511/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 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0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22073064 +##$YMIN_a= -11385727 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/511/fid b/Extracellular/DDvsSD/SD_Stage2/511/fid new file mode 100644 index 0000000000000000000000000000000000000000..205c53397a344a12110074bfe804adce59777be4 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/511/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..03c12b68522144939b173d8da3635e754a59d9fd Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..d02ebb03c15a2ead3d39bf1c886d742ad8a21719 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8404 +##$PC= 1 +##$PHC0= -25.25208 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908751045 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 275243750 +##$YMIN_p= -59866 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/title b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..0f9ccdf682a27622f5981e3b1dfbb8de04f6b1cb --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/511/pdata/1/title @@ -0,0 +1 @@ +511, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage2/511/pulseprogram b/Extracellular/DDvsSD/SD_Stage2/511/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/511/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage2/512/acqu b/Extracellular/DDvsSD/SD_Stage2/512/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/512/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 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0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 21981915 +##$YMIN_a= -11624956 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/512/fid b/Extracellular/DDvsSD/SD_Stage2/512/fid new file mode 100644 index 0000000000000000000000000000000000000000..1f07ce7fe495384cd53d5b9ee142077c3039eb5d Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/512/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..556f7f166467340864103c5c17b8dd5b9a5f5673 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..d4260278056eb1233b2d107ab880695138b6976a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84039 +##$PC= 1 +##$PHC0= -25.82336 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908754547 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 537660728 +##$YMIN_p= -129821 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/title b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..359aeaa02085d9626cf73872a81af8750e629a18 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/512/pdata/1/title @@ -0,0 +1 @@ +512, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage2/512/pulseprogram b/Extracellular/DDvsSD/SD_Stage2/512/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/512/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage2/513/acqu b/Extracellular/DDvsSD/SD_Stage2/513/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/513/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 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120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 20877318 +##$YMIN_a= -11128608 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/513/fid b/Extracellular/DDvsSD/SD_Stage2/513/fid new file mode 100644 index 0000000000000000000000000000000000000000..1bafd24081c380c83c21a5bba7592256d40bafa1 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/513/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..78ff7505d91a7a18d81412a48aa8a8bc50d6e39d Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..ddc530b97bed8f58fdb32d99ca0684ec3b0fac1f --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84023 +##$PC= 1 +##$PHC0= -25.90576 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908871475 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 508153735 +##$YMIN_p= -130912 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/title b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f66704273135235df7d35493508de66c17175aae --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/513/pdata/1/title @@ -0,0 +1 @@ +513, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage2/513/pulseprogram b/Extracellular/DDvsSD/SD_Stage2/513/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage2/513/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage3/.DS_Store b/Extracellular/DDvsSD/SD_Stage3/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..1b383fc817bb8946a19801da69ec4ca59fb490bf Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/.DS_Store differ diff --git a/Extracellular/DDvsSD/SD_Stage3/611/acqu b/Extracellular/DDvsSD/SD_Stage3/611/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/611/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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0000000000000000000000000000000000000000..75781968c6a65cf9cd6232de92f2517e8b976e11 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/611/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..ee2bb4ae1005eb876cb991c968e79f9cf5044573 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..f5009162dbae2108cf24bdb2ea322b49ef750721 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84013 +##$PC= 1 +##$PHC0= -25.32898 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908942894 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 529779777 +##$YMIN_p= -105719 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/title b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..04d0b3dc7c09ee6f98cd9d2f1c02fc1207c4826a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/611/pdata/1/title @@ -0,0 +1 @@ +611, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage3/611/pulseprogram b/Extracellular/DDvsSD/SD_Stage3/611/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/611/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage3/612/acqu b/Extracellular/DDvsSD/SD_Stage3/612/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/612/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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0000000000000000000000000000000000000000..95c2d9a87317b1327378a29120e9011b33b912a3 Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/612/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..365f31638b7c3863b2328d288338033c94b82edd Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..9aa8cc5664ca0009efefa14f94e48dc542052f52 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83999 +##$PC= 1 +##$PHC0= -25.86731 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909039513 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 515675961 +##$YMIN_p= -114264 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/title b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..80827673d0bbb91ff3d6c679fbefdd723c8e2457 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/612/pdata/1/title @@ -0,0 +1 @@ +612, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage3/612/pulseprogram b/Extracellular/DDvsSD/SD_Stage3/612/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/612/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/SD_Stage3/613/acqu b/Extracellular/DDvsSD/SD_Stage3/613/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/613/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence 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0000000000000000000000000000000000000000..0d67da828b9658a648c35115fbe7ab1ecddcc4ab Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/613/fid differ diff --git a/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/1r b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..eeb62db20a2400fb53d76b8e9f225564fa87d25b Binary files /dev/null and b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/proc b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/procs b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..c0c5d73c91f643f897c91038eed7f16b3c28c028 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84029 +##$PC= 1 +##$PHC0= -25.48279 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908825264 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 285349481 +##$YMIN_p= -62177 +##END= diff --git a/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/title b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..8fc70a0705a3e368a53ec815102344ce20e92529 --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/613/pdata/1/title @@ -0,0 +1 @@ +613, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/SD_Stage3/613/pulseprogram b/Extracellular/DDvsSD/SD_Stage3/613/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/SD_Stage3/613/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/Undifferentiated/.DS_Store b/Extracellular/DDvsSD/Undifferentiated/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..dd488887fb1a8e3fd98b0ff42e7cd16befac9817 Binary files /dev/null and b/Extracellular/DDvsSD/Undifferentiated/.DS_Store differ diff --git a/Extracellular/DDvsSD/Undifferentiated/901/acqu b/Extracellular/DDvsSD/Undifferentiated/901/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/901/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/procs b/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..2fbf75888cdd86db54ff561a0b4fc2a204379f63 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 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+##$NZP= 0 +##$OFFSET= 19.84156 +##$PC= 1 +##$PHC0= -25.36743 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169907937447 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 455314585 +##$YMIN_p= -89129 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/title b/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..4ea2e66a9e72923a528b89a5beea2c83cc6cdb93 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/901/pdata/1/title @@ -0,0 +1 @@ +901, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/Undifferentiated/901/pulseprogram b/Extracellular/DDvsSD/Undifferentiated/901/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/901/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/Undifferentiated/902/acqu b/Extracellular/DDvsSD/Undifferentiated/902/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/902/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 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b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/1r differ diff --git a/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/proc b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> 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+##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/procs b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..64a69f6d9dcfc97ceaede4509e961e407621258e --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84121 +##$PC= 1 +##$PHC0= -25.48828 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990818531 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 348550364 +##$YMIN_p= -105725 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/title b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..84db2d4e539b8e238d6b5e57d527d8752f7f8d71 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/902/pdata/1/title @@ -0,0 +1 @@ +902, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/Undifferentiated/902/pulseprogram b/Extracellular/DDvsSD/Undifferentiated/902/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/902/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/Undifferentiated/903/acqu b/Extracellular/DDvsSD/Undifferentiated/903/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/903/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 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b/Extracellular/DDvsSD/Undifferentiated/903/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84078 +##$PC= 1 +##$PHC0= -25.69153 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908484978 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 409016891 +##$YMIN_p= -81092 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/903/pdata/1/title b/Extracellular/DDvsSD/Undifferentiated/903/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..6bed75799c2adbebfb2e9bedcda55d99ead18d5f --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/903/pdata/1/title @@ -0,0 +1 @@ +903, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/Undifferentiated/903/pulseprogram b/Extracellular/DDvsSD/Undifferentiated/903/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/903/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/Undifferentiated/904/acqu b/Extracellular/DDvsSD/Undifferentiated/904/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/904/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ 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+##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84031 +##$PC= 1 +##$PHC0= -25.06531 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908816162 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 335029994 +##$YMIN_p= -74920 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/904/pdata/1/title b/Extracellular/DDvsSD/Undifferentiated/904/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..88e4be104f126e3eb40da32ef76c5e08ac76c6e2 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/904/pdata/1/title @@ -0,0 +1 @@ +904, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/Undifferentiated/904/pulseprogram b/Extracellular/DDvsSD/Undifferentiated/904/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/904/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/Undifferentiated/905/acqu b/Extracellular/DDvsSD/Undifferentiated/905/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/905/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= 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a/Extracellular/DDvsSD/Undifferentiated/905/pdata/1/procs b/Extracellular/DDvsSD/Undifferentiated/905/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..a1fd1d28641c2440f2c99561c8dc232247b14946 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/905/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 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+##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 404539968 +##$YMIN_p= -100967 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/905/pdata/1/title b/Extracellular/DDvsSD/Undifferentiated/905/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..88e812c69e3cb9b2617b9972aaf3c8d52023a650 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/905/pdata/1/title @@ -0,0 +1 @@ +905, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/Undifferentiated/905/pulseprogram b/Extracellular/DDvsSD/Undifferentiated/905/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/905/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/DDvsSD/Undifferentiated/906/acqu b/Extracellular/DDvsSD/Undifferentiated/906/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/906/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 +##$DE= 55 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 12 +##$DQDMODE= 0 +##$DR= 22 +##$DS= 4 +##$DSPFIRM= 4 +##$DSPFVS= 0 +##$DTYPA= 0 +##$EXP= +##$FCUCHAN= (0..9) +0 2 0 0 0 0 0 0 0 0 +##$FL1= 90 +##$FL2= 90 +##$FL3= 90 +##$FL4= 90 +##$FN_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$FOV= 20 +##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= 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+##$LOCKFLD= 0 +##$LOCKGN= 0 +##$LOCKPOW= -20 +##$LOCKPPM= 0 +##$LOCNUC= <2H> +##$LOCPHAS= 0 +##$LOCSHFT= no +##$LOCSW= 0 +##$LTIME= 0.1 +##$MASR= 4200 +##$MASRLST= +##$MULEXPNO= (0..15) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$NBL= 1 +##$NC= 0 +##$NLOGCH= 2 +##$NOVFLW= 0 +##$NS= 32 +##$NUC1= <1H> +##$NUC2= +##$NUC3= +##$NUC4= +##$NUC5= +##$NUC6= +##$NUC7= +##$NUC8= +##$NUCLEUS= +##$NUSLIST= +##$NusAMOUNT= 25 +##$NusFPNZ= no +##$NusJSP= 0 +##$NusSEED= 54321 +##$NusSPTYPE= 0 +##$NusT2= 1 +##$NusTD= 0 +##$O1= 3296.2 +##$O2= 3297.086 +##$O3= 3297.086 +##$O4= 3297.086 +##$O5= 3297.086 +##$O6= 3297.086 +##$O7= 3297.086 +##$O8= 3297.086 +##$OVERFLW= 0 +##$P= (0..63) +21.06 21.06 42.12 0 0 16.5 25 50 20000 0 0 80000 80000 1000 0 0 1000 2500 +100000 600 0 0 0 0 0 72 100000 21.06 0 1000 0 0 20000 0 0 0 0 0 0 0 2000 +0 0 0 171 0 80000 46600 10000 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PACOIL= (0..15) +1 4 0 0 2 3 0 0 0 0 0 0 0 0 0 0 +##$PAPS= 2 +##$PARMODE= 0 +##$PCPD= (0..9) +100 65 80 100 100 100 100 100 100 100 +##$PEXSEL= (0..9) +1 1 1 1 1 1 1 1 1 1 +##$PHCOR= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PHLIST= <> +##$PHP= 1 +##$PH_ref= 0 +##$PL= (0..63) +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 +##$PLSTEP= 0.1 +##$PLSTRT= -6 +##$PLW= (0..63) +0 5.7 0 0 0 0 0 0 0 2.528085e-05 4.0465 0.39516 0 0 0 0 0 0 5.7 0.59859 +0 0 0 0 0 0 0 1.9514 0 4.0465 0 0 4.0465e-06 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PLWMAX= (0..7) +0 0 0 0 0 0 0 0 +##$PQPHASE= 0 +##$PQSCALE= 1 +##$PR= 1 +##$PRECHAN= (0..15) +-1 4 0 1 5 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$PRGAIN= 0 +##$PROBHD= <> +##$PULPROG= +##$PW= 0 +##$PYNM= +##$ProjAngle= 0 +##$QNP= 1 +##$RD= 0 +##$RECCHAN= (0..15) +0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECPH= 0 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100644 index 0000000000000000000000000000000000000000..461c3effa68c4c5343ef4a548d1980fb140071d9 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/906/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 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b/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/procs b/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..30ca52d2e213eba5e000faefe4b6315e879459f9 --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8418 +##$PC= 1 +##$PHC0= -25.92773 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169907770103 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 481940051 +##$YMIN_p= -94753 +##END= diff --git a/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/title b/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..9548751e25e2a0cb797fc5d7661717073e68c33f --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/906/pdata/1/title @@ -0,0 +1 @@ +906, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/DDvsSD/Undifferentiated/906/pulseprogram b/Extracellular/DDvsSD/Undifferentiated/906/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/DDvsSD/Undifferentiated/906/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/.DS_Store b/Extracellular/SD/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..5918f3d9f94e92c65a8fc922f7b1d0b5f90aefdd Binary files /dev/null and b/Extracellular/SD/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage1/.DS_Store b/Extracellular/SD/SD_Stage1/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..8eddadee93588512dad978838c148165d8375ebf Binary files /dev/null and b/Extracellular/SD/SD_Stage1/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage1/411/acqu b/Extracellular/SD/SD_Stage1/411/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/411/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= 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120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= 0 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1/411/acqus b/Extracellular/SD/SD_Stage1/411/acqus new file mode 100644 index 0000000000000000000000000000000000000000..eede83488cefa62e2d552e73fca552d4f7424d02 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/411/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie 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+##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8398 +##$PC= 1 +##$PHC0= -24.81262 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909167648 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 313642930 +##$YMIN_p= -68872 +##END= diff --git a/Extracellular/SD/SD_Stage1/411/pdata/1/title b/Extracellular/SD/SD_Stage1/411/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..27af325fb683373b43ff15680ab86810370aef18 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/411/pdata/1/title @@ -0,0 +1 @@ +411, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1/411/pulseprogram b/Extracellular/SD/SD_Stage1/411/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/411/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1/412/acqu b/Extracellular/SD/SD_Stage1/412/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/412/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 +##$DE= 55 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 12 +##$DQDMODE= 0 +##$DR= 22 +##$DS= 4 +##$DSPFIRM= 4 +##$DSPFVS= 0 +##$DTYPA= 0 +##$EXP= 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+##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= 0 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1/412/acqus b/Extracellular/SD/SD_Stage1/412/acqus new file mode 100644 index 0000000000000000000000000000000000000000..bfbed09592ddc50812f7fc67e4beb27f7fa7a050 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/412/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 1624915395 +##$DE= 56.70621 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 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120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22375399 +##$YMIN_a= -11893983 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1/412/fid b/Extracellular/SD/SD_Stage1/412/fid new file mode 100644 index 0000000000000000000000000000000000000000..95119c90e1633fce24f0acfbe73b0843500213ea Binary files /dev/null and b/Extracellular/SD/SD_Stage1/412/fid differ diff --git a/Extracellular/SD/SD_Stage1/412/pdata/1/1r b/Extracellular/SD/SD_Stage1/412/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..3fecbee3562d57fac6010b8a9b995e8327b3abc0 Binary files /dev/null and b/Extracellular/SD/SD_Stage1/412/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage1/412/pdata/1/proc b/Extracellular/SD/SD_Stage1/412/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/412/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1/412/pdata/1/procs b/Extracellular/SD/SD_Stage1/412/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..30a06a0dae85843fee7485ac713519f75e114c38 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/412/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83948 +##$PC= 1 +##$PHC0= -25.7135 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909394501 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 272378567 +##$YMIN_p= -61077 +##END= diff --git a/Extracellular/SD/SD_Stage1/412/pdata/1/title b/Extracellular/SD/SD_Stage1/412/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..b732b1769fe8a766f7473667b4c4984212bf0e96 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/412/pdata/1/title @@ -0,0 +1 @@ +412, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1/412/pulseprogram b/Extracellular/SD/SD_Stage1/412/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/412/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1/413/acqu b/Extracellular/SD/SD_Stage1/413/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/413/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 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+##$PLSTEP= 0.1 +##$PLSTRT= -6 +##$PLW= (0..63) +0 5.7 0 0 0 0 0 0 0 2.506522e-05 4.0107 0.39167 0 0 0 0 0 0 5.7 0.5933 +0 0 0 0 0 0 0 1.9342 0 4.0107 0 0 4.0107e-06 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PLWMAX= (0..7) +63.6 0 0 0 0 0 0 0 +##$PQPHASE= 0 +##$PQSCALE= 1 +##$PR= 1 +##$PRECHAN= (0..15) +-1 4 0 1 5 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$PRGAIN= 0 +##$PROBHD= +##$PULPROG= +##$PW= 0 +##$PYNM= +##$ProjAngle= 0 +##$QNP= 1 +##$RD= 0 +##$RECCHAN= (0..15) +0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECPH= 0 +##$RECPRE= (0..15) +-1 0 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$RECPRFX= (0..15) +1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECSEL= (0..15) +0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RG= 56.72 +##$RO= 0 +##$RSEL= (0..15) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$S= (0..7) +83 4 83 83 83 83 83 83 +##$SELREC= (0..9) +0 0 0 0 0 0 0 0 0 0 +##$SFO1= 700.1732962 +##$SFO2= 700.173297086 +##$SFO3= 700.173297086 +##$SFO4= 700.173297086 +##$SFO5= 700.173297086 +##$SFO6= 700.173297086 +##$SFO7= 700.173297086 +##$SFO8= 700.173297086 +##$SOLVENT= +##$SOLVOLD= +##$SP= (0..63) +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 +##$SPECTR= 0 +##$SPINCNT= 0 +##$SPNAM= (0..63) +<> <> + <> <> <> + <> <> + <> <> <> <> <> <> +<> <> <> <> <> <> +<> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> +##$SPOAL= (0..63) +0.5 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +1 1 1 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 +##$SPOFFS= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPPEX= (0..63) +0 0 0 0 0 0 0 0 0 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0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 20803518 +##$YMIN_a= -10853788 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1/413/fid b/Extracellular/SD/SD_Stage1/413/fid new file mode 100644 index 0000000000000000000000000000000000000000..8b9d8246be3ce587879bce69dc2301f80c3f0687 Binary files /dev/null and b/Extracellular/SD/SD_Stage1/413/fid differ diff --git a/Extracellular/SD/SD_Stage1/413/pdata/1/1r b/Extracellular/SD/SD_Stage1/413/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..97912e0ebe95a4bdc0fd8d98985ec8d393fff8f3 Binary files /dev/null and b/Extracellular/SD/SD_Stage1/413/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage1/413/pdata/1/proc b/Extracellular/SD/SD_Stage1/413/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/413/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1/413/pdata/1/procs b/Extracellular/SD/SD_Stage1/413/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..f2725bde1cc34236c2160aae01f6c789e94e46a1 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/413/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83958 +##$PC= 1 +##$PHC0= -25.10925 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909321686 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 515098398 +##$YMIN_p= -120903 +##END= diff --git a/Extracellular/SD/SD_Stage1/413/pdata/1/title b/Extracellular/SD/SD_Stage1/413/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..86defa883c35926b421e697829d8e477016b4dda --- /dev/null +++ b/Extracellular/SD/SD_Stage1/413/pdata/1/title @@ -0,0 +1 @@ +413, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1/413/pulseprogram b/Extracellular/SD/SD_Stage1/413/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/413/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 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b/Extracellular/SD/SD_Stage1/414/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/414/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1/414/pdata/1/procs b/Extracellular/SD/SD_Stage1/414/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..62434009287d30b5fc38608a709c04e2a155361e --- /dev/null +++ b/Extracellular/SD/SD_Stage1/414/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83935 +##$PC= 1 +##$PHC0= -25.3125 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909487625 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 269565943 +##$YMIN_p= -66570 +##END= diff --git a/Extracellular/SD/SD_Stage1/414/pdata/1/title b/Extracellular/SD/SD_Stage1/414/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..bedb36d25dff6bebe2031a0db2b30ff589cdd83a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/414/pdata/1/title @@ -0,0 +1 @@ +414, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1/414/pulseprogram b/Extracellular/SD/SD_Stage1/414/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/414/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1/415/acqu b/Extracellular/SD/SD_Stage1/415/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/415/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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+##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 19198485 +##$YMIN_a= -10206999 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1/415/fid b/Extracellular/SD/SD_Stage1/415/fid new file mode 100644 index 0000000000000000000000000000000000000000..e4c976a549331ec18a4d968952a1708dd6074b01 Binary files /dev/null and b/Extracellular/SD/SD_Stage1/415/fid differ diff --git a/Extracellular/SD/SD_Stage1/415/pdata/1/1r b/Extracellular/SD/SD_Stage1/415/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..34afea22b4da9e66176f4530785705e517090b22 Binary files /dev/null and b/Extracellular/SD/SD_Stage1/415/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage1/415/pdata/1/proc b/Extracellular/SD/SD_Stage1/415/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/415/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1/415/pdata/1/procs b/Extracellular/SD/SD_Stage1/415/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..54db6f827ab2674da5e151e1bb90fbbd4085c07e --- /dev/null +++ b/Extracellular/SD/SD_Stage1/415/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83945 +##$PC= 1 +##$PHC0= -25.3894 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909416908 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 457661231 +##$YMIN_p= -105595 +##END= diff --git a/Extracellular/SD/SD_Stage1/415/pdata/1/title b/Extracellular/SD/SD_Stage1/415/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..756283c7a9cbe96ed7cf012f02b540ec0326495b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/415/pdata/1/title @@ -0,0 +1 @@ +415, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1/415/pulseprogram b/Extracellular/SD/SD_Stage1/415/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/415/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1/416/acqu b/Extracellular/SD/SD_Stage1/416/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/416/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 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0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0716e-05 9.207e-06 0 0 0.0071955 2.4954e-05 0 2.4954e-07 0 0.0071955 +0.0071955 0 0 0 0 0 0 0 1.469701e-05 2.284603e-05 1.066748e-05 5.752882e-05 +0 0 0 0 0 0 0.095318 5.4617 0 0 0 0.00010066 9.207e-06 0.00058925 0 0 0 +0 2.4954e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.2001 +##$TE1= 300.2001 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 28782291 +##$YMIN_a= -15044678 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1/416/fid b/Extracellular/SD/SD_Stage1/416/fid new file mode 100644 index 0000000000000000000000000000000000000000..163e1c9199c9970d45f82698f985106d63f3d81c Binary files /dev/null and b/Extracellular/SD/SD_Stage1/416/fid differ diff --git a/Extracellular/SD/SD_Stage1/416/pdata/1/1r b/Extracellular/SD/SD_Stage1/416/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..08103c2ba87c66c8c88579657168941c8186e898 Binary files /dev/null and b/Extracellular/SD/SD_Stage1/416/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage1/416/pdata/1/proc b/Extracellular/SD/SD_Stage1/416/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1/416/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1/416/pdata/1/procs b/Extracellular/SD/SD_Stage1/416/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..839c4cb589e353e5203dffeac5d13ede9dda6afc --- /dev/null +++ b/Extracellular/SD/SD_Stage1/416/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83935 +##$PC= 1 +##$PHC0= -25.76294 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909486221 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 318126917 +##$YMIN_p= -89740 +##END= diff --git a/Extracellular/SD/SD_Stage1/416/pdata/1/title b/Extracellular/SD/SD_Stage1/416/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..643b476b3f17c24ef8d7b50b6f7f23acc72ee76a --- /dev/null +++ b/Extracellular/SD/SD_Stage1/416/pdata/1/title @@ -0,0 +1 @@ +416, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1/416/pulseprogram b/Extracellular/SD/SD_Stage1/416/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1/416/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/.DS_Store b/Extracellular/SD/SD_Stage1_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..f308f5e3feb765f85e521e312c9d10fd16617f4d Binary files /dev/null and b/Extracellular/SD/SD_Stage1_CellFreeControl/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/acqu b/Extracellular/SD/SD_Stage1_CellFreeControl/431/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/431/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) 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0 0 0 0 +##$TDav= 1 +##$TE= 300.2005 +##$TE1= 300.2005 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 22847276 +##$YMIN_a= -12026849 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/fid b/Extracellular/SD/SD_Stage1_CellFreeControl/431/fid new file mode 100644 index 0000000000000000000000000000000000000000..e43903c6290b033115dd484601b8e79057ee5798 Binary files /dev/null and b/Extracellular/SD/SD_Stage1_CellFreeControl/431/fid differ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/1r b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..3b325bc8b83ddb99b441549ea0b17209f8dc2407 Binary files /dev/null and b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/proc b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/procs b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..289e01f13170fda2399458d73120bd1d8f2d3638 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83621 +##$PC= 1 +##$PHC0= -25.31799 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169911681953 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 295480845 +##$YMIN_p= -59821 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/title b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..77c90f8015474fe27bccdca65f491c10b592a72a --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pdata/1/title @@ -0,0 +1 @@ +431, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/431/pulseprogram b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/431/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/432/acqu b/Extracellular/SD/SD_Stage1_CellFreeControl/432/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/432/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 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0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/procs b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..7259fc2be8eafb12d9a6dc3b63f2fd12f48bba65 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 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+##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83979 +##$PC= 1 +##$PHC0= -25.16418 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909175346 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 505501619 +##$YMIN_p= -113313 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/title b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..310833fc970ac4f1b14428f889ac9232b22e6e5f --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pdata/1/title @@ -0,0 +1 @@ +432, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/432/pulseprogram b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/432/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/433/acqu b/Extracellular/SD/SD_Stage1_CellFreeControl/433/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/433/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 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files /dev/null and b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/proc b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 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+##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/procs b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..4c49cb2145a974fcd966a7f56d6c5645644dc6a7 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83966 +##$PC= 1 +##$PHC0= -25.0708 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909271271 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 492777724 +##$YMIN_p= -95293 +##END= diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/title b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..dcc747cf648609b444328eedb0b7c3da8bb92f16 --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pdata/1/title @@ -0,0 +1 @@ +433, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage1_CellFreeControl/433/pulseprogram b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage1_CellFreeControl/433/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage2/.DS_Store b/Extracellular/SD/SD_Stage2/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..57077b97e701da3c4dd1127f008542ab527d3c3d Binary files /dev/null and b/Extracellular/SD/SD_Stage2/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage2/511/acqu b/Extracellular/SD/SD_Stage2/511/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage2/511/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number 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0000000000000000000000000000000000000000..d02ebb03c15a2ead3d39bf1c886d742ad8a21719 --- /dev/null +++ b/Extracellular/SD/SD_Stage2/511/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8404 +##$PC= 1 +##$PHC0= -25.25208 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908751045 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 275243750 +##$YMIN_p= -59866 +##END= diff --git a/Extracellular/SD/SD_Stage2/511/pdata/1/title b/Extracellular/SD/SD_Stage2/511/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..0f9ccdf682a27622f5981e3b1dfbb8de04f6b1cb --- /dev/null +++ b/Extracellular/SD/SD_Stage2/511/pdata/1/title @@ -0,0 +1 @@ +511, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage2/511/pulseprogram b/Extracellular/SD/SD_Stage2/511/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage2/511/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage2/512/acqu b/Extracellular/SD/SD_Stage2/512/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage2/512/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) 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+##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84039 +##$PC= 1 +##$PHC0= -25.82336 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908754547 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 537660728 +##$YMIN_p= -129821 +##END= diff --git a/Extracellular/SD/SD_Stage2/512/pdata/1/title b/Extracellular/SD/SD_Stage2/512/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..359aeaa02085d9626cf73872a81af8750e629a18 --- /dev/null +++ b/Extracellular/SD/SD_Stage2/512/pdata/1/title @@ -0,0 +1 @@ +512, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage2/512/pulseprogram b/Extracellular/SD/SD_Stage2/512/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage2/512/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage2/513/acqu b/Extracellular/SD/SD_Stage2/513/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage2/513/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 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sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84023 +##$PC= 1 +##$PHC0= -25.90576 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908871475 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 508153735 +##$YMIN_p= -130912 +##END= diff --git a/Extracellular/SD/SD_Stage2/513/pdata/1/title b/Extracellular/SD/SD_Stage2/513/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f66704273135235df7d35493508de66c17175aae --- /dev/null +++ b/Extracellular/SD/SD_Stage2/513/pdata/1/title @@ -0,0 +1 @@ +513, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage2/513/pulseprogram b/Extracellular/SD/SD_Stage2/513/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage2/513/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/.DS_Store b/Extracellular/SD/SD_Stage2_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..07180bb1a6c7d0132ce9243407c06f3fa7735e0e Binary files /dev/null and b/Extracellular/SD/SD_Stage2_CellFreeControl/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/532/acqu b/Extracellular/SD/SD_Stage2_CellFreeControl/532/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/532/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH 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--git a/Extracellular/SD/SD_Stage2_CellFreeControl/532/pdata/1/procs b/Extracellular/SD/SD_Stage2_CellFreeControl/532/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..25cd230448b652250f281360b4f4ca0a685be4c8 --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/532/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84011 +##$PC= 1 +##$PHC0= -25.51575 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990895269 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 520393105 +##$YMIN_p= -111748 +##END= diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/532/pdata/1/title b/Extracellular/SD/SD_Stage2_CellFreeControl/532/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..912eeb4a4453b6370dd42cfc3d4f241e1dca4ced --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/532/pdata/1/title @@ -0,0 +1 @@ +532, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/532/pulseprogram b/Extracellular/SD/SD_Stage2_CellFreeControl/532/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/532/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/533/acqu b/Extracellular/SD/SD_Stage2_CellFreeControl/533/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- 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<1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/533/pdata/1/procs b/Extracellular/SD/SD_Stage2_CellFreeControl/533/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..5c529a4e7b2fac5ea2d7af52bcfc399d7f56d6c8 --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/533/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 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+##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84012 +##$PC= 1 +##$PHC0= -24.80713 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908945694 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 509724178 +##$YMIN_p= -119655 +##END= diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/533/pdata/1/title b/Extracellular/SD/SD_Stage2_CellFreeControl/533/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..9590d0850ef46350c031f7f6ec37e3c06939b16b --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/533/pdata/1/title @@ -0,0 +1 @@ +533, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage2_CellFreeControl/533/pulseprogram b/Extracellular/SD/SD_Stage2_CellFreeControl/533/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage2_CellFreeControl/533/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage3/.DS_Store b/Extracellular/SD/SD_Stage3/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..1b383fc817bb8946a19801da69ec4ca59fb490bf Binary files /dev/null and b/Extracellular/SD/SD_Stage3/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage3/611/acqu b/Extracellular/SD/SD_Stage3/611/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage3/611/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 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index 0000000000000000000000000000000000000000..ee2bb4ae1005eb876cb991c968e79f9cf5044573 Binary files /dev/null and b/Extracellular/SD/SD_Stage3/611/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage3/611/pdata/1/proc b/Extracellular/SD/SD_Stage3/611/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage3/611/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 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+##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage3/611/pdata/1/procs b/Extracellular/SD/SD_Stage3/611/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..f5009162dbae2108cf24bdb2ea322b49ef750721 --- /dev/null +++ b/Extracellular/SD/SD_Stage3/611/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84013 +##$PC= 1 +##$PHC0= -25.32898 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908942894 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 529779777 +##$YMIN_p= -105719 +##END= diff --git a/Extracellular/SD/SD_Stage3/611/pdata/1/title b/Extracellular/SD/SD_Stage3/611/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..04d0b3dc7c09ee6f98cd9d2f1c02fc1207c4826a --- /dev/null +++ b/Extracellular/SD/SD_Stage3/611/pdata/1/title @@ -0,0 +1 @@ +611, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage3/611/pulseprogram b/Extracellular/SD/SD_Stage3/611/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage3/611/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage3/612/acqu b/Extracellular/SD/SD_Stage3/612/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage3/612/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 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0000000000000000000000000000000000000000..365f31638b7c3863b2328d288338033c94b82edd Binary files /dev/null and b/Extracellular/SD/SD_Stage3/612/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage3/612/pdata/1/proc b/Extracellular/SD/SD_Stage3/612/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage3/612/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage3/612/pdata/1/procs b/Extracellular/SD/SD_Stage3/612/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..9aa8cc5664ca0009efefa14f94e48dc542052f52 --- /dev/null +++ b/Extracellular/SD/SD_Stage3/612/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.83999 +##$PC= 1 +##$PHC0= -25.86731 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169909039513 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 515675961 +##$YMIN_p= -114264 +##END= diff --git a/Extracellular/SD/SD_Stage3/612/pdata/1/title b/Extracellular/SD/SD_Stage3/612/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..80827673d0bbb91ff3d6c679fbefdd723c8e2457 --- /dev/null +++ b/Extracellular/SD/SD_Stage3/612/pdata/1/title @@ -0,0 +1 @@ +612, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage3/612/pulseprogram b/Extracellular/SD/SD_Stage3/612/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage3/612/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage3/613/acqu b/Extracellular/SD/SD_Stage3/613/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage3/613/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 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0 0 0 0 0 0 +##$FOV= 20 +##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GRDPROG= <> +##$GRPDLY= -1 +##$HDDUTY= 20 +##$HDRATE= 1 +##$HGAIN= (0..3) +0 0 0 0 +##$HL1= 1 +##$HL2= 35 +##$HL3= 16 +##$HL4= 17 +##$HOLDER= 304 +##$HPMOD= (0..7) +0 0 0 0 0 0 0 0 +##$HPPRGN= 0 +##$IN= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$INF= (0..7) +0 0 0 0 0 0 0 0 +##$INP= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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+##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 0 +##$YMIN_a= 0 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage3/613/acqus b/Extracellular/SD/SD_Stage3/613/acqus new file mode 100644 index 0000000000000000000000000000000000000000..fc110f5c9e904f602822d63bb63d4d7e72eb739b --- /dev/null +++ b/Extracellular/SD/SD_Stage3/613/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 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-1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84029 +##$PC= 1 +##$PHC0= -25.48279 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908825264 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 285349481 +##$YMIN_p= -62177 +##END= diff --git a/Extracellular/SD/SD_Stage3/613/pdata/1/title b/Extracellular/SD/SD_Stage3/613/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..8fc70a0705a3e368a53ec815102344ce20e92529 --- /dev/null +++ b/Extracellular/SD/SD_Stage3/613/pdata/1/title @@ -0,0 +1 @@ +613, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage3/613/pulseprogram b/Extracellular/SD/SD_Stage3/613/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage3/613/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/.DS_Store b/Extracellular/SD/SD_Stage3_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..9d47b72023214d1298d8511a6275872973bc04d7 Binary files /dev/null and b/Extracellular/SD/SD_Stage3_CellFreeControl/.DS_Store differ diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/631/acqu b/Extracellular/SD/SD_Stage3_CellFreeControl/631/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/631/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) 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+##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84073 +##$PC= 1 +##$PHC0= -24.73022 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908515785 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 327170184 +##$YMIN_p= -64068 +##END= diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/631/pdata/1/title b/Extracellular/SD/SD_Stage3_CellFreeControl/631/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..4a1261070e73ecd07db39702f230d84f71f675ec --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/631/pdata/1/title @@ -0,0 +1 @@ +631, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/631/pulseprogram b/Extracellular/SD/SD_Stage3_CellFreeControl/631/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/631/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/632/acqu b/Extracellular/SD/SD_Stage3_CellFreeControl/632/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/632/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 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b/Extracellular/SD/SD_Stage3_CellFreeControl/632/acqus new file mode 100644 index 0000000000000000000000000000000000000000..5e8c5fd723375d60eb0f2d0fd8333850ee921a0b --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/632/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 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0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/procs b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..579e97452ad78982d142499ca9ab8f3d5058c795 --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84092 +##$PC= 1 +##$PHC0= -25.41687 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908388359 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 428760132 +##$YMIN_p= -89241 +##END= diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/title b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..f56adb97abea57023be4aea5bce3999bb756a30e --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pdata/1/title @@ -0,0 +1 @@ +632, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/632/pulseprogram b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/632/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/acqu b/Extracellular/SD/SD_Stage3_CellFreeControl/633/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/633/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 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120 120 120 +##$PLSTEP= 0.1 +##$PLSTRT= -6 +##$PLW= (0..63) +0 5.7 0 0 0 0 0 0 0 2.501745e-05 4.0021 0.39083 0 0 0 0 0 0 5.7 0.59203 +0 0 0 0 0 0 0 1.93 0 4.0021 0 0 4.0021e-06 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$PLWMAX= (0..7) +63.6 0 0 0 0 0 0 0 +##$PQPHASE= 0 +##$PQSCALE= 1 +##$PR= 1 +##$PRECHAN= (0..15) +-1 4 0 1 5 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$PRGAIN= 0 +##$PROBHD= +##$PULPROG= +##$PW= 0 +##$PYNM= +##$ProjAngle= 0 +##$QNP= 1 +##$RD= 0 +##$RECCHAN= (0..15) +0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECPH= 0 +##$RECPRE= (0..15) +-1 0 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 -1 +##$RECPRFX= (0..15) +1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RECSEL= (0..15) +0 0 1 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$RG= 56.72 +##$RO= 0 +##$RSEL= (0..15) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$S= (0..7) +83 4 83 83 83 83 83 83 +##$SELREC= (0..9) +0 0 0 0 0 0 0 0 0 0 +##$SFO1= 700.1732962 +##$SFO2= 700.173297086 +##$SFO3= 700.173297086 +##$SFO4= 700.173297086 +##$SFO5= 700.173297086 +##$SFO6= 700.173297086 +##$SFO7= 700.173297086 +##$SFO8= 700.173297086 +##$SOLVENT= +##$SOLVOLD= +##$SP= (0..63) +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 +##$SPECTR= 0 +##$SPINCNT= 0 +##$SPNAM= (0..63) +<> <> + <> <> <> + <> <> + <> <> <> <> <> <> +<> <> <> <> <> <> +<> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> +##$SPOAL= (0..63) +0.5 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +1 1 1 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 +##$SPOFFS= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPPEX= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0765e-05 9.2288e-06 0 0 0.0072125 2.5013e-05 0 2.5013e-07 0 0.0072125 +0.0072125 0 0 0 0 0 0 0 1.473133e-05 2.289937e-05 1.069238e-05 5.766314e-05 +0 0 0 0 0 0 0.095543 5.4747 0 0 0 0.00010089 9.2288e-06 0.00059064 0 0 +0 0 2.5013e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.1918 +##$TE1= 300.1918 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 23171221 +##$YMIN_a= -11714602 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/fid b/Extracellular/SD/SD_Stage3_CellFreeControl/633/fid new file mode 100644 index 0000000000000000000000000000000000000000..c411818fc016ac076a718c4b255410263f858e71 Binary files /dev/null and b/Extracellular/SD/SD_Stage3_CellFreeControl/633/fid differ diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/1r b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..9a0267653190f6a69b5a964c938045de82a4507e Binary files /dev/null and b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/1r differ diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/proc b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/procs b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..5ff387d3e3487947557b666bf18231cfc1bb0341 --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -1 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84085 +##$PC= 1 +##$PHC0= -24.92249 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908432465 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 268657016 +##$YMIN_p= -62073 +##END= diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/title b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..1efb1a892fec98b68e5e2eeb2e0996aed87f63f0 --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pdata/1/title @@ -0,0 +1 @@ +633, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/SD/SD_Stage3_CellFreeControl/633/pulseprogram b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/SD/SD_Stage3_CellFreeControl/633/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/.DS_Store b/Extracellular/Undifferentiated/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..4364f5a1d7ce1d1ea5fec5100b0b37e724ee35e7 Binary files /dev/null and b/Extracellular/Undifferentiated/.DS_Store differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/.DS_Store b/Extracellular/Undifferentiated/Undifferentiated/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..dd488887fb1a8e3fd98b0ff42e7cd16befac9817 Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated/.DS_Store differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/acqu b/Extracellular/Undifferentiated/Undifferentiated/901/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/901/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 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700.173297086 +##$SFO7= 700.173297086 +##$SFO8= 700.173297086 +##$SOLVENT= +##$SOLVOLD= +##$SP= (0..63) +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 120 +120 120 120 120 120 120 120 120 120 120 +##$SPECTR= 0 +##$SPINCNT= 0 +##$SPNAM= (0..63) +<> <> + <> <> <> + <> <> + <> <> <> <> <> <> +<> <> <> <> <> <> +<> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> <> +##$SPOAL= (0..63) +0.5 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +1 1 1 1 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 +0.5 0.5 0.5 0.5 0.5 0.5 0.5 +##$SPOFFS= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPPEX= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SPW= (0..63) +0 2.0384e-05 9.0594e-06 0 0 0.0070801 2.4554e-05 0 2.4554e-07 0 0.0070801 +0.0070801 0 0 0 0 0 0 0 1.44609e-05 2.2479e-05 1.04961e-05 5.66046e-05 +0 0 0 0 0 0 0.09379 5.3742 0 0 0 9.9042e-05 9.0594e-06 0.0005798 0 0 0 +0 2.4554e-07 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SUBNAM= (0..9) +<> <> <> <> <> <> <> <> <> <> +##$SW= 30.0045766888882 +##$SWIBOX= (0..19) +0 0 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$SW_h= 21008.4033613445 +##$SWfinal= 0 +##$SigLockShift= 0 +##$TD= 65536 +##$TD0= 1 +##$TD_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$TDav= 1 +##$TE= 300.2007 +##$TE1= 300.2007 +##$TE2= 0 +##$TE3= 0 +##$TE4= 0 +##$TEG= 300 +##$TE_MAGNET= 0 +##$TE_PIDX= 1 +##$TE_STAB= (0..9) +1 1 0 0 0 0 0 0 0 0 +##$TL= (0..7) +0 120 120 120 120 120 120 120 +##$TOTROT= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$TUBE_TYPE= <> +##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 19696423 +##$YMIN_a= -10364047 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/fid b/Extracellular/Undifferentiated/Undifferentiated/901/fid new file mode 100644 index 0000000000000000000000000000000000000000..4ded997c1ba6f1490368d19d2570ad22b4600948 Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated/901/fid differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/1r b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..6edb0c770114f017a3633ce0e0d111b39ae883b4 Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/1r differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/proc b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..2fbf75888cdd86db54ff561a0b4fc2a204379f63 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84156 +##$PC= 1 +##$PHC0= -25.36743 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169907937447 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 455314585 +##$YMIN_p= -89129 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..4ea2e66a9e72923a528b89a5beea2c83cc6cdb93 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/901/pdata/1/title @@ -0,0 +1 @@ +901, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated/901/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated/901/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/901/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated/902/acqu b/Extracellular/Undifferentiated/Undifferentiated/902/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/902/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 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b/Extracellular/Undifferentiated/Undifferentiated/902/fid new file mode 100644 index 0000000000000000000000000000000000000000..f3e52e96d6b99072928f8c6c1c039c2031ebf8f7 Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated/902/fid differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/1r b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..44e3aa1f95406ee947aa50292b35caf510f07838 Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/1r differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/proc b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..64a69f6d9dcfc97ceaede4509e961e407621258e --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84121 +##$PC= 1 +##$PHC0= -25.48828 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.16990818531 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 348550364 +##$YMIN_p= -105725 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..84db2d4e539b8e238d6b5e57d527d8752f7f8d71 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/902/pdata/1/title @@ -0,0 +1 @@ +902, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated/902/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated/902/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/902/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated/903/acqu b/Extracellular/Undifferentiated/Undifferentiated/903/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/903/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 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b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/1r differ diff --git a/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/proc b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..0a9dd3b0e9ceaf164362d0ce11e1ea74083e4748 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84078 +##$PC= 1 +##$PHC0= -25.69153 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908484978 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 409016891 +##$YMIN_p= -81092 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..6bed75799c2adbebfb2e9bedcda55d99ead18d5f --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/903/pdata/1/title @@ -0,0 +1 @@ +903, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated/903/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated/903/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/903/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated/904/acqu b/Extracellular/Undifferentiated/Undifferentiated/904/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/904/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 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1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/904/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated/904/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..43f0a039c10d9488c4ad0b2d8a45ad1d899bb5af --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/904/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84031 +##$PC= 1 +##$PHC0= -25.06531 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908816162 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 335029994 +##$YMIN_p= -74920 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/904/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated/904/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..88e4be104f126e3eb40da32ef76c5e08ac76c6e2 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/904/pdata/1/title @@ -0,0 +1 @@ +904, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated/904/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated/904/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/904/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git 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+##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/905/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated/905/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..a1fd1d28641c2440f2c99561c8dc232247b14946 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/905/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84149 +##$PC= 1 +##$PHC0= -24.9884 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169907985062 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 404539968 +##$YMIN_p= -100967 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/905/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated/905/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..88e812c69e3cb9b2617b9972aaf3c8d52023a650 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/905/pdata/1/title @@ -0,0 +1 @@ +905, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated/905/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated/905/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/905/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated/906/acqu b/Extracellular/Undifferentiated/Undifferentiated/906/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/906/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 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1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/906/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated/906/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..30ca52d2e213eba5e000faefe4b6315e879459f9 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/906/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.8418 +##$PC= 1 +##$PHC0= -25.92773 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169907770103 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 481940051 +##$YMIN_p= -94753 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated/906/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated/906/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..9548751e25e2a0cb797fc5d7661717073e68c33f --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/906/pdata/1/title @@ -0,0 +1 @@ +906, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated/906/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated/906/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated/906/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/.DS_Store b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/.DS_Store new file mode 100644 index 0000000000000000000000000000000000000000..cdf582be187ffb7210b4e5219fc6ea2c782e954d Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/.DS_Store differ diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/acqu b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$BYTORDA= 0 +##$CAGPARS= (0..11) +0 0 0 0 0 0 0 0 0 0 0 0 +##$CHEMSTR= +##$CNST= (0..63) +1 1 145 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.75 1 1 1 +1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 +##$CPDPRG= (0..8) +<> <> <> <> +##$D= (0..63) +0 4 0 0 0 0 0 0 0.01 0.06 0 0.03 2e-05 0 0 0 0.0002 0 0 0 0.0003 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 +##$DATE= 0 +##$DE= 55 +##$DECBNUC= +##$DECIM= 952 +##$DECNUC= +##$DECSTAT= 4 +##$DIGMOD= 3 +##$DIGTYP= 12 +##$DQDMODE= 0 +##$DR= 22 +##$DS= 4 +##$DSPFIRM= 4 +##$DSPFVS= 0 +##$DTYPA= 0 +##$EXP= +##$FCUCHAN= (0..9) +0 2 0 0 0 0 0 0 0 0 +##$FL1= 90 +##$FL2= 90 +##$FL3= 90 +##$FL4= 90 +##$FN_INDIRECT= (0..7) +0 0 0 0 0 0 0 0 +##$FOV= 20 +##$FQ1LIST= +##$FQ2LIST= +##$FQ3LIST= +##$FQ4LIST= +##$FQ5LIST= +##$FQ6LIST= +##$FQ7LIST= +##$FQ8LIST= +##$FRQLO3= 0 +##$FRQLO3N= 0 +##$FS= (0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GRDPROG= <> +##$GRPDLY= -1 +##$HDDUTY= 20 +##$HDRATE= 1 +##$HGAIN= (0..3) +0 0 0 0 +##$HL1= 1 +##$HL2= 35 +##$HL3= 16 +##$HL4= 17 +##$HOLDER= 304 +##$HPMOD= (0..7) +0 0 0 0 0 0 0 0 +##$HPPRGN= 0 +##$IN= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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+##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908213318 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 374191936 +##$YMIN_p= -66705 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..68bc1f73d64cf945a0a178b61b6b8c34a4e6512e --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/pdata/1/title @@ -0,0 +1 @@ +911, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/911/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/acqu b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 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+##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84101 +##$PC= 1 +##$PHC0= -25.21912 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908323242 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 332168308 +##$YMIN_p= -54592 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..c8244f41de1b5f1ba03fdc565dceee0b2e6715e2 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/pdata/1/title @@ -0,0 +1 @@ +912, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/912/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $ diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/acqu b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/acqu new file mode 100644 index 0000000000000000000000000000000000000000..da4c645a88085da5c1b2cf8cc51cdf7be80ba36a --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/acqu @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 30 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= 1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= <> +##$AUTOPOS= <> +##$BF1= 700.17 +##$BF2= 700.17 +##$BF3= 700.17 +##$BF4= 700.17 +##$BF5= 700.17 +##$BF6= 700.17 +##$BF7= 700.17 +##$BF8= 700.17 +##$BWFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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(0..7) +83 83 83 83 83 83 83 83 +##$FTLPGN= 0 +##$FW= 4032000 +##$FnILOOP= 0 +##$FnMODE= 0 +##$FnTYPE= 0 +##$GPNAM= (0..31) + + + + + + +##$GPX= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPY= (0..31) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GPZ= (0..31) +0 50 -10 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$GRDPROG= <> +##$GRPDLY= -1 +##$HDDUTY= 20 +##$HDRATE= 1 +##$HGAIN= (0..3) +0 0 0 0 +##$HL1= 1 +##$HL2= 35 +##$HL3= 16 +##$HL4= 17 +##$HOLDER= 304 +##$HPMOD= (0..7) +0 0 0 0 0 0 0 0 +##$HPPRGN= 0 +##$IN= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$INF= (0..7) +0 0 0 0 0 0 0 0 +##$INP= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$INSTRUM= <> +##$INTEGFAC= (0..63) +0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 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+##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/acqus b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/acqus new file mode 100644 index 0000000000000000000000000000000000000000..ede7369c3604c85bc6d378963c4be4a8dee0f272 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/acqus @@ -0,0 +1,329 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 14 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ACQT0= 0 +##$AMP= (0..31) +100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 +100 100 100 100 100 100 100 100 100 100 100 100 100 100 +##$AMPCOIL= (0..19) +-1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 +##$ANAVPT= -1 +##$AQSEQ= 0 +##$AQ_mod= 3 +##$AUNM= +##$AUTOPOS= <> +##$BF1= 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+##$USERA1= <> +##$USERA2= <> +##$USERA3= <> +##$USERA4= <> +##$USERA5= <> +##$V9= 5 +##$VALIDCODE= -1 +##$VALIST= <> +##$VCLIST= <> +##$VDLIST= <> +##$VPLIST= <> +##$VTLIST= <> +##$WBST= 1024 +##$WBSW= 8 +##$XGAIN= (0..3) +0 0 0 0 +##$XL= 0 +##$YL= 0 +##$YMAX_a= 14983787 +##$YMIN_a= -8492499 +##$ZGOPTNS= <-DFLAG_BLK> +##$ZL1= 120 +##$ZL2= 120 +##$ZL3= 120 +##$ZL4= 120 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/fid b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/fid new file mode 100644 index 0000000000000000000000000000000000000000..c94340676f51dcaeea950452fd05d086c21482b5 Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/fid differ diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/1r b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/1r new file mode 100644 index 0000000000000000000000000000000000000000..afd579243dcd0616e07642d00c16b8552e6af90c Binary files /dev/null and b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/1r differ diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/proc b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/proc new file mode 100644 index 0000000000000000000000000000000000000000..22e8821512f0ff8e2f7d6e6ec1d61b4f3048bae6 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/proc @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 17 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 14.95061 +##$ABSF2= -5.471745 +##$ABSG= 1 +##$ABSL= 5 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 1 +##$BC_mod= 2 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 2 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 0 +##$GAMMA= 1 +##$GB= 0.01 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 23 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0.8 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 1 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= yes +##$Mdd_CsZF= 2 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= 0 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 1 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 14.70929 +##$PC= 1 +##$PHC0= -25.46082 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.17 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.H2O+D2O> +##$SSB= 2 +##$STSI= 0 +##$STSR= 0 +##$SW_p= 14005.6022408964 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 0 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 0 +##$YMIN_p= 0 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/procs b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/procs new file mode 100644 index 0000000000000000000000000000000000000000..e4d4f0d111126c2257e1d34beacc87ec81d1ec95 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/procs @@ -0,0 +1,139 @@ +##TITLE= Parameter file, TopSpin 3.5 pl 6 +##JCAMPDX= 5.0 +##DATATYPE= Parameter Values +##NPOINTS= 9 $$ modification sequence number +##ORIGIN= Bruker BioSpin GmbH +##OWNER= Marie Phelan, University of Liverpool +$$ +$$ +$$ +##$ABSF1= 0 +##$ABSF2= 0 +##$ABSG= 0 +##$ABSL= 0 +##$ALPHA= 0 +##$AQORDER= 0 +##$ASSFAC= 0 +##$ASSFACI= 0 +##$ASSFACX= 0 +##$ASSWID= 0 +##$AUNMP= +##$AXLEFT= 0 +##$AXNAME= <> +##$AXNUC= <1H> +##$AXRIGHT= 0 +##$AXTYPE= 0 +##$AXUNIT= <> +##$AZFE= 0.1 +##$AZFW= 0.1 +##$BCFW= 0 +##$BC_mod= 0 +##$BYTORDP= 0 +##$COROFFS= 0 +##$CY= 100 +##$DATMOD= 1 +##$DC= 0 +##$DFILT= <> +##$DTYPP= 0 +##$ERETIC= no +##$F1P= 5.3 +##$F2P= 4.9 +##$FCOR= 0.5 +##$FTSIZE= 131072 +##$FT_mod= 6 +##$GAMMA= 0 +##$GB= 0 +##$INTBC= 1 +##$INTSCL= 1 +##$ISEN= 128 +##$LB= 0.3 +##$LEV0= 0 +##$LPBIN= 0 +##$MAXI= 1000 +##$MC2= 0 +##$MEAN= 0 +##$ME_mod= 0 +##$MI= 2 +##$MddCEXP= no +##$MddCT_SP= no +##$MddF180= no +##$MddLAMBDA= 0 +##$MddMEMORY= 0 +##$MddMERGE= 0 +##$MddNCOMP= 0 +##$MddNITER= 0 +##$MddNOISE= 0 +##$MddPHASE= 0 +##$MddSEED= 0 +##$MddSRSIZE= 0 +##$Mdd_CsALG= 0 +##$Mdd_CsLAMBDA= 0 +##$Mdd_CsNITER= 0 +##$Mdd_CsNORM= 0 +##$Mdd_CsVE= no +##$Mdd_CsZF= 0 +##$Mdd_LrLAMBDA= 0 +##$Mdd_LrNITER= 0 +##$Mdd_LrRANK= 0 +##$Mdd_LrZF= 0 +##$Mdd_mod= 0 +##$NCOEF= 0 +##$NC_proc= -2 +##$NLEV= 6 +##$NOISF1= 7.934625 +##$NOISF2= 7.601621 +##$NSP= 0 +##$NTH_PI= 0 +##$NZP= 0 +##$OFFSET= 19.84103 +##$PC= 1 +##$PHC0= -25.00488 +##$PHC1= 0 +##$PH_mod= 1 +##$PKNL= yes +##$PPARMOD= 0 +##$PPDIAG= 0 +##$PPIPTYP= 0 +##$PPMPNUM= 100 +##$PPRESOL= 1 +##$PSCAL= 1 +##$PSIGN= 0 +##$PYNMP= +##$RDF1= 0 +##$RDF2= 0 +##$RDFWHM= 0 +##$RDINT= 0 +##$RDPOS= 0 +##$REVERSE= no +##$SF= 700.169908307838 +##$SI= 131072 +##$SIGF1= 9 +##$SIGF2= 5 +##$SINO= 0 +##$SIOLD= 131072 +##$SPECTYP= <> +##$SREF_mod= 1 +##$SREGLST= <1H.CDCl3> +##$SSB= 0 +##$STSI= 131072 +##$STSR= 0 +##$SW_p= 21008.4033613445 +##$SYMM= 0 +##$S_DEV= 0 +##$TDeff= 65536 +##$TDoff= 0 +##$TI= <> +##$TILT= no +##$TM1= 0 +##$TM2= 0 +##$TOPLEV= 0 +##$USERP1= <> +##$USERP2= <> +##$USERP3= <> +##$USERP4= <> +##$USERP5= <> +##$WDW= 1 +##$XDIM= 0 +##$YMAX_p= 282913416 +##$YMIN_p= -39864 +##END= diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/title b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/title new file mode 100644 index 0000000000000000000000000000000000000000..2d5991285e76b3bf66a6b75c2266fded9f9e9646 --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pdata/1/title @@ -0,0 +1 @@ +913, IPSC study, Cell Media, R Oldershaw diff --git a/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pulseprogram b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pulseprogram new file mode 100644 index 0000000000000000000000000000000000000000..d0945a28855ebd5571d447fb0cfa3dfbc3f96e7b --- /dev/null +++ b/Extracellular/Undifferentiated/Undifferentiated_CellFreeControl/913/pulseprogram @@ -0,0 +1,184 @@ +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;cpmgpr1d +;avance-version (12/01/11) +;1D experiment with +; T2 filter using Carr-Purcell-Meiboom-Gill sequence +;using f1 presaturation +; +;$CLASS=HighRes +;$DIM=1D +;$TYPE= +;$SUBTYPE= +;$COMMENT= + + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" 1 +;Avance3.incl +; for AV III +; +;avance-version (13/06/17) +; +;$CLASS=HighRes Incl +;$COMMENT= +# 169 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Avance.incl" +;$Id: Avance3.incl,v 1.10.2.2 2013/08/30 09:43:33 ber Exp $ +# 14 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + +# 1 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" 1 +;Delay.incl - include file for commonly used delays +; +;version (13/08/07) +; +;$CLASS=HighRes Incl +;$COMMENT= + +# 9 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;general delays + +define delay DELTA +define delay DELTA1 +define delay DELTA2 +define delay DELTA3 +define delay DELTA4 +define delay DELTA5 +define delay DELTA6 +define delay DELTA7 +define delay DELTA8 +define delay DELTA9 +define delay DELTA10 +define delay DELTA11 +define delay DELTA12 +define delay DELTA13 +define delay DELTA14 +define delay DELTA15 +define delay DELTA16 + +define delay TAU +define delay TAU1 +define delay TAU2 +define delay TAU3 +define delay TAU4 +define delay TAU5 +define delay TAU6 +define delay TAU7 +define delay TAU8 +define delay TAU9 +# 40 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay INCR1 +define delay INCR2 +define delay INCR3 +define delay INCR4 +define delay INCR5 +define delay INCR6 + + +;delays for centering pulses +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define delay CEN_HN1 +define delay CEN_HN2 +define delay CEN_HN3 +define delay CEN_HC1 +define delay CEN_HC2 +define delay CEN_HC3 +define delay CEN_HC4 +define delay CEN_HP1 +define delay CEN_HP2 +define delay CEN_CN1 +define delay CEN_CN2 +define delay CEN_CN3 +define delay CEN_CN4 +define delay CEN_CP1 +define delay CEN_CP2 + + +;loop counters +# 69 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +define loopcounter COUNTER +define loopcounter SCALEF +define loopcounter FACTOR1 +define loopcounter FACTOR2 +define loopcounter FACTOR3 +define loopcounter FACTOR4 +define loopcounter FACTOR5 +define loopcounter FACTOR6 + + +# 80 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/Delay.incl" +;$Id: Delay.incl,v 1.14.2.1 2013/08/30 09:43:33 ber Exp $ +# 15 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" 2 + + +# 18 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"p2=p1*2" +"d11=30m" +"d12=20u" + + +"DELTA1=d20-p1*2/3.1416" +"DELTA2=d20-de" +# 27 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +"acqt0=0" +baseopt_echo + + +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. part of mc cmd. before ze" +; dimension 1D; AQ_mode +define delay MCWRK +define delay MCREST +"MCREST = 30m - 30m" +"MCWRK = 0.333333*30m" + + dccorr +# 31 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +1 ze +# 1 "mc_line 31 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. def. of mc cmd. after ze" +# 32 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +# 1 "mc_line 32 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. start label for mc cmd." +2 MCWRK * 2 +LBLF0, MCWRK + MCREST +# 33 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" + d12 pl9:f1 + d1 cw:f1 ph29 + 4u do:f1 + d12 pl1:f1 + p1 ph1 + DELTA1 + p2 ph2 + d20 +3 d20 + p2 ph2 + d20 + lo to 3 times l4 + d20 + p2 ph2 + DELTA2 + go=2 ph31 +# 1 "mc_line 49 file /opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d exp. mc cmd. in line" + MCWRK wr #0 + MCWRK zd + lo to LBLF0 times td0 + +# 50 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +exit +# 53 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +ph1=0 0 2 2 1 1 3 3 +ph2=1 3 1 3 0 2 0 2 +ph29=0 +ph31=0 0 2 2 1 1 3 3 + + +;pl1 : f1 channel - power level for pulse (default) +;pl9 : f1 channel - power level for presaturation +;p1 : f1 channel - 90 degree high power pulse +;p2 : f1 channel - 180 degree high power pulse +;d1 : relaxation delay; 1-5 * T1 +;d11: delay for disk I/O [30 msec] +;d12: delay for power switching [20 usec] +;d20: fixed echo time to allow elimination of J-mod. effects +; d20 should be << 1/J ,but > (50 * P2) [1-2 msec] +;l4: loop for T2 filter [4 - 20] +;ns: 1 * n, total number of scans: NS * TD0 +;ds: 16 +# 74 "/opt/topspin3.5pl6/exp/stan/nmr/lists/pp/cpmgpr1d" +;$Id: cpmgpr1d,v 1.8 2012/01/31 17:49:22 ber Exp $